2-(4-carboxylphenyl)-5-(10-bromodecyl)-1,3,2-dioxaborinane

Base Information

Chemical Name:2-(4-carboxylphenyl)-5-(10-bromodecyl)-1,3,2-dioxaborinane
CAS No.:147633-38-3
Molecular Formula:C₂₀H₃₀BBrO₄
Molecular Weight:425.171
Hs Code.:

Synonyms:2-(4-carboxylphenyl)-5-(10-bromodecyl)-1,3,2-dioxaborinane

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Chemical Property of 2-(4-carboxylphenyl)-5-(10-bromodecyl)-1,3,2-dioxaborinane

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Technology Process of 2-(4-carboxylphenyl)-5-(10-bromodecyl)-1,3,2-dioxaborinane

There total 1 articles about 2-(4-carboxylphenyl)-5-(10-bromodecyl)-1,3,2-dioxaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 14047-29-1
4-carboxyphenylboronic acid

: 133997-03-2
2-(10-bromodecyl)-1,3-propanediol

: 147633-38-3
2-(4-carboxylphenyl)-5-(10-bromodecyl)-1,3,2-dioxaborinane

Guidance literature:: In toluene; byproducts: H2O; refluxing (2 h), cooling to room temp.; collection by filtration;
DOI:10.1246/bcsj.66.578

Reference yield: 69.0%

: 147633-38-3
2-(4-carboxylphenyl)-5-(10-bromodecyl)-1,3,2-dioxaborinane

: 1565-80-6
(2S)-2-methyl-1-butanol

: 2-(4-{(S)-2-methylbutoxycarbonyl}phenyl)-5-(10-bromodecyl)-1,3,2-dioxaborinane

Guidance literature:: With sulfuric acid; In benzene; refluxing in presence of H2SO4 (5 h); solvent evapn., chromy. (silica, CH2Cl2), recrystn. (hexane);
DOI:10.1246/bcsj.66.578

Reference yield: 52.0%

: 147633-38-3
2-(4-carboxylphenyl)-5-(10-bromodecyl)-1,3,2-dioxaborinane

: 85394-10-1
<(S)-2-methyl-1-butyl> p-hydroxybenzoate

: 2-{4-{4-{(S)-2-methylbutoxycarbonyl}phenoxycarbonyl}phenyl}-5-(10-bromodecyl)-1,3,2-dioxaborinane

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; In tetrahydrofuran; pyridine; 1,2-dichloro-ethane; refluxing of B-compd. with SOCl2 in presence of DMF in C2H4Cl2 (1 h), solvent removal (reduced pressure), dissolving in THF, dropwise addn. to soln. of org. compd. in pyridine (0°C), stirring (room temp., 20 h); solvent evapn., extn. (ether), washing (water), drying (Na2SO4), concn., chromy. (silica, hexane/CH2Cl2), recrystn. (hexane);
DOI:10.1246/bcsj.66.578