5,8-dibromo-2-(4-((2-ethylhexyl)oxy)phenyl)-1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole

Base Information

• Chemical Name: 5,8-dibromo-2-(4-((2-ethylhexyl)oxy)phenyl)-1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole
• CAS No.: 1375171-39-3
• Molecular Formula: C₃₁H₃₆Br₂N₂OS₂
• Molecular Weight: 676.58

Synonyms:5,8-dibromo-2-(4-((2-ethylhexyl)oxy)phenyl)-1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole

Chemical Property of 5,8-dibromo-2-(4-((2-ethylhexyl)oxy)phenyl)-1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole

Chemical Property:

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Technology Process of 5,8-dibromo-2-(4-((2-ethylhexyl)oxy)phenyl)-1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole

There total 3 articles about 5,8-dibromo-2-(4-((2-ethylhexyl)oxy)phenyl)-1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.4%

2-(4-((2-ethylhexyl)oxy)phenyl)-1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole (1375171-36-0) → 5,8-dibromo-2-(4-((2-ethylhexyl)oxy)phenyl)-1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole (1375171-39-3)

Guidance literature:

With N-Bromosuccinimide; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/ol300867e

Reference yield:

benzo[1,2-b:4,3-b’]dithiophene-4,5-quinone (24243-31-0) → 5,8-dibromo-2-(4-((2-ethylhexyl)oxy)phenyl)-1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole (1375171-39-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: ammonium acetate; acetic acid / 100 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 95 °C

2.2: 20 - 95 °C

3.1: N-Bromosuccinimide / tetrahydrofuran / 20 °C

With N-Bromosuccinimide; ammonium acetate; potassium carbonate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/ol300867e

Reference yield:

4-[(2-ethylhexyl)oxy]benzaldehyde (119630-71-6) → 5,8-dibromo-2-(4-((2-ethylhexyl)oxy)phenyl)-1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole (1375171-39-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: ammonium acetate; acetic acid / 100 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 95 °C

2.2: 20 - 95 °C

3.1: N-Bromosuccinimide / tetrahydrofuran / 20 °C

With N-Bromosuccinimide; ammonium acetate; potassium carbonate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/ol300867e

upstream raw materials:

2-(4-((2-ethylhexyl)oxy)phenyl)-1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole

benzo[1,2-b:4,3-b’]dithiophene-4,5-quinone

4-[(2-ethylhexyl)oxy]benzaldehyde

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