4-chloro-2,7-bis-(2,6-diisopropyl-phenyl)-9-(6-hydroxy-hexylamino)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Base Information

• Chemical Name: 4-chloro-2,7-bis-(2,6-diisopropyl-phenyl)-9-(6-hydroxy-hexylamino)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone
• CAS No.: 894788-68-2
• Molecular Formula: C₄₄H₅₀ClN₃O₅
• Molecular Weight: 736.351

Synonyms:4-chloro-2,7-bis-(2,6-diisopropyl-phenyl)-9-(6-hydroxy-hexylamino)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Chemical Property of 4-chloro-2,7-bis-(2,6-diisopropyl-phenyl)-9-(6-hydroxy-hexylamino)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

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Technology Process of 4-chloro-2,7-bis-(2,6-diisopropyl-phenyl)-9-(6-hydroxy-hexylamino)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

There total 1 articles about 4-chloro-2,7-bis-(2,6-diisopropyl-phenyl)-9-(6-hydroxy-hexylamino)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

6-amino-1-hexanol (4048-33-3) + N,N'-di-(2',6'-diisopropylphenyl)-2,6-dichloronaphthalene-1,4,5,8-tetracarboxylic acid bisimide (485831-66-1) → 4-chloro-2,7-bis-(2,6-diisopropyl-phenyl)-9-(6-hydroxy-hexylamino)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone (894788-68-2)

Guidance literature:

In chloroform; at 20 ℃; for 5h;

DOI:10.1021/ja0584469

Reference yield: 54.0%

4-chloro-2,7-bis-(2,6-diisopropyl-phenyl)-9-(6-hydroxy-hexylamino)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone (894788-68-2) + 3,5-didodecyloxybenzoic acid (123126-40-9)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/ja0584469

Reference yield:

4-chloro-2,7-bis-(2,6-diisopropyl-phenyl)-9-(6-hydroxy-hexylamino)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone (894788-68-2) + tert-butylchlorodiphenylsilane (58479-61-1) → C60H68ClN3O5Si (1027338-55-1)

Guidance literature:

With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/ja710253q

upstream raw materials:

6-amino-1-hexanol

N,N'-di-(2',6'-diisopropylphenyl)-2,6-dichloronaphthalene-1,4,5,8-tetracarboxylic acid bisimide

Downstream raw materials:

3,5-bis-dodecyloxy-benzoic acid 6-[2,7-bis-(2,6-diisopropyl-phenyl)-9-(6-hydroxy-hexylamino)-1,3,6,8-tetraoxo-1,2,3,6,7,8-hexahydro-benzo[lmn][3,8]phenanthrolin-4-ylamino]-hexyl ester

C₆₀H₆₈ClN₃O₅Si

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