4-[(chloro)(fluoro)methyl]-3-methyl-1-phenyl-6,7-dihydro-1H-pyrazolo[3,4 b]pyridin-6-one

Base Information

Chemical Name:4-[(chloro)(fluoro)methyl]-3-methyl-1-phenyl-6,7-dihydro-1H-pyrazolo[3,4 b]pyridin-6-one
CAS No.:1350908-63-2
Molecular Formula:C₁₄H₁₁ClFN₃O
Molecular Weight:291.712
Hs Code.:

Synonyms:4-[(chloro)(fluoro)methyl]-3-methyl-1-phenyl-6,7-dihydro-1H-pyrazolo[3,4 b]pyridin-6-one

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Chemical Property of 4-[(chloro)(fluoro)methyl]-3-methyl-1-phenyl-6,7-dihydro-1H-pyrazolo[3,4 b]pyridin-6-one

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Technology Process of 4-[(chloro)(fluoro)methyl]-3-methyl-1-phenyl-6,7-dihydro-1H-pyrazolo[3,4 b]pyridin-6-one

There total 1 articles about 4-[(chloro)(fluoro)methyl]-3-methyl-1-phenyl-6,7-dihydro-1H-pyrazolo[3,4 b]pyridin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1131-18-6
1-Phenyl-3-methyl-5-aminopyrazole

: 111218-58-7
ethyl 4-chloro-4-fluoro-3-oxobutanoate

: 1350908-63-2
4-[(chloro)(fluoro)methyl]-3-methyl-1-phenyl-6,7-dihydro-1H-pyrazolo[3,4 b]pyridin-6-one

Guidance literature:: In acetic acid; for 3h; Reflux;
DOI:10.1007/s11172-011-0114-y

Reference yield: 89.0%

: 1350908-63-2
4-[(chloro)(fluoro)methyl]-3-methyl-1-phenyl-6,7-dihydro-1H-pyrazolo[3,4 b]pyridin-6-one

: 108-98-5
thiophenol

: 1350908-55-2
C₂₀H₁₆FN₃OS

Guidance literature:: thiophenol; With sodium hydride; In N,N-dimethyl-formamide; at 50 ℃;

4-[(chloro)(fluoro)methyl]-3-methyl-1-phenyl-6,7-dihydro-1H-pyrazolo[3,4 b]pyridin-6-one; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1007/s11172-011-0114-y

Reference yield: 85.0%

: 1350908-63-2
4-[(chloro)(fluoro)methyl]-3-methyl-1-phenyl-6,7-dihydro-1H-pyrazolo[3,4 b]pyridin-6-one

: 106-54-7
p-Chlorothiophenol

: 1350908-56-3
C₂₀H₁₅ClFN₃OS

Guidance literature:: p-Chlorothiophenol; With sodium hydride; In N,N-dimethyl-formamide;

4-[(chloro)(fluoro)methyl]-3-methyl-1-phenyl-6,7-dihydro-1H-pyrazolo[3,4 b]pyridin-6-one; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1007/s11172-011-0114-y