1,2-bis(p-methylphenyl)-2-tosylethanol

Base Information

Chemical Name:1,2-bis(p-methylphenyl)-2-tosylethanol
CAS No.:647864-31-1
Molecular Formula:C₂₃H₂₄O₃S
Molecular Weight:380.508
Hs Code.:

Synonyms:1,2-bis(p-methylphenyl)-2-tosylethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bis(p-methylphenyl)-2-tosylethanol

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Technology Process of 1,2-bis(p-methylphenyl)-2-tosylethanol

There total 1 articles about 1,2-bis(p-methylphenyl)-2-tosylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 21668-99-5
1-methyl-4-((4-methylbenzyl)sulfonyl)benzene

: 104-87-0
4-methyl-benzaldehyde

: 647864-31-1
1,2-bis(p-methylphenyl)-2-tosylethanol

Guidance literature:: 1-methyl-4-((4-methylbenzyl)sulfonyl)benzene; With n-butyllithium; In tetrahydrofuran; hexane; for 1h;

4-methyl-benzaldehyde; In tetrahydrofuran; hexane; at -40 ℃; for 4h;
DOI:10.1021/ol0357954

Reference yield: 87.0%

: 647864-31-1
1,2-bis(p-methylphenyl)-2-tosylethanol

: 1,2-bis(p-methylphenyl)vinyl p-tolyl sulfone

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/ol0357954

Reference yield:

: 647864-31-1
1,2-bis(p-methylphenyl)-2-tosylethanol

: 3,6-dimethyl-9-tosylphenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / mesyl chloride; triethylamine / CH₂Cl₂ / 24 h / 20 °C

2: 80 percent / I₂ / tetrahydrofuran / Irradiation

With iodine; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0357954