sodium (E)-4-(3-(4-chlorophenyl)-3-oxoprop-1-en-1-yl)-2-methoxyphenyl sulfate

Base Information

Chemical Name:sodium (E)-4-(3-(4-chlorophenyl)-3-oxoprop-1-en-1-yl)-2-methoxyphenyl sulfate
CAS No.:1352508-89-4
Molecular Formula:C₁₆H₁₂ClO₆S*Na
Molecular Weight:390.776
Hs Code.:

Synonyms:sodium (E)-4-(3-(4-chlorophenyl)-3-oxoprop-1-en-1-yl)-2-methoxyphenyl sulfate

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Chemical Property of sodium (E)-4-(3-(4-chlorophenyl)-3-oxoprop-1-en-1-yl)-2-methoxyphenyl sulfate

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Technology Process of sodium (E)-4-(3-(4-chlorophenyl)-3-oxoprop-1-en-1-yl)-2-methoxyphenyl sulfate

There total 3 articles about sodium (E)-4-(3-(4-chlorophenyl)-3-oxoprop-1-en-1-yl)-2-methoxyphenyl sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: (E)-1-(4-chlorophenyl)-3-(3-methoxy-4-(hydroxy)phenyl)prop-2-en-1-one

: 1352508-89-4
sodium (E)-4-(3-(4-chlorophenyl)-3-oxoprop-1-en-1-yl)-2-methoxyphenyl sulfate

Guidance literature:: (E)-1-(4-chlorophenyl)-3-(3-methoxy-4-(hydroxy)phenyl)prop-2-en-1-one; With pyridine; chlorosulfonic acid; at -10 - 20 ℃; Inert atmosphere;

With sodium hydroxide; In ethanol; water; Inert atmosphere;
DOI:10.1021/ml200017d

Reference yield:

: 5533-00-6
3-methoxy-4-methoxymethoxy-benzaldehyde

: 1352508-89-4
sodium (E)-4-(3-(4-chlorophenyl)-3-oxoprop-1-en-1-yl)-2-methoxyphenyl sulfate

Guidance literature:: Multi-step reaction with 3 steps

1.1: baryte hydrate / 10 h / 20 °C

2.1: hydrogenchloride / tetrahydrofuran; water / 0.5 h / 60 °C

3.1: pyridine; chlorosulfonic acid / -10 - 20 °C / Inert atmosphere

3.2: Inert atmosphere

With pyridine; hydrogenchloride; chlorosulfonic acid; In tetrahydrofuran; water; 1.1: Claisen Schmidt reaction;
DOI:10.1021/ml200017d

Reference yield:

: 99-91-2
para-chloroacetophenone

: 1352508-89-4
sodium (E)-4-(3-(4-chlorophenyl)-3-oxoprop-1-en-1-yl)-2-methoxyphenyl sulfate

Guidance literature:: Multi-step reaction with 3 steps

1.1: baryte hydrate / 10 h / 20 °C

2.1: hydrogenchloride / tetrahydrofuran; water / 0.5 h / 60 °C

3.1: pyridine; chlorosulfonic acid / -10 - 20 °C / Inert atmosphere

3.2: Inert atmosphere

With pyridine; hydrogenchloride; chlorosulfonic acid; In tetrahydrofuran; water; 1.1: Claisen Schmidt reaction;
DOI:10.1021/ml200017d