C₂₄H₃₄O₆S

Base Information

Chemical Name:C₂₄H₃₄O₆S
CAS No.:1389395-08-7
Molecular Formula:C₂₄H₃₄O₆S
Molecular Weight:450.596
Hs Code.:

C<sub>24</sub>H<sub>34</sub>O<sub>6</sub>S

Synonyms:C₂₄H₃₄O₆S

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Chemical Property of C₂₄H₃₄O₆S

Chemical Property:

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Technology Process of C₂₄H₃₄O₆S

There total 4 articles about C₂₄H₃₄O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1389395-07-6
C₁₇H₂₈O₄

: 98-59-9
p-toluenesulfonyl chloride

: 1389395-08-7
C₂₄H₃₄O₆S

Guidance literature:: With 1-methyl-1H-imidazole; triethylamine; lithium chloride; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1055/s-0031-1290803

Reference yield:

: 1389394-98-2
(E)-methyl 3-oxo-7-(tosyloxy)oct-6-enoate

: 1389395-08-7
C₂₄H₃₄O₆S

Guidance literature:: Multi-step reaction with 9 steps

1: 1-methyl-1H-imidazole; triethylamine; lithium chloride / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / hexane; N,N-dimethyl-formamide / 23 h / 50 °C / Inert atmosphere

3: methanesulfonamide / water; tert-butyl alcohol / 16.5 h / 0 - 20 °C

4: pyridine / dichloromethane / 4 h / 0 - 20 °C

5: potassium carbonate / methanol / 1.5 h / 20 °C

6: lithium aluminium tetrahydride / diethyl ether / 2 h / -40 - 0 °C

7: 1H-imidazole; carbon tetrabromide; triphenylphosphine / dichloromethane / 0.5 h / 0 °C

8: n-butyllithium; sodium hydride / tetrahydrofuran / 1 h / 0 °C

9: 1-methyl-1H-imidazole; triethylamine; lithium chloride / dichloromethane / 3 h / 20 °C

With pyridine; 1H-imidazole; 1-methyl-1H-imidazole; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium aluminium tetrahydride; n-butyllithium; carbon tetrabromide; methanesulfonamide; sodium hydride; potassium carbonate; triethylamine; triphenylphosphine; lithium chloride; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 2: Negishi coupling reaction;
DOI:10.1055/s-0031-1290803

Reference yield:

: 1389395-00-9
(2Z,6E)-methyl 3,7-bis(tosyloxy)octa-2,6-dienoate

: 1389395-08-7
C₂₄H₃₄O₆S

Guidance literature:: Multi-step reaction with 8 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / hexane; N,N-dimethyl-formamide / 23 h / 50 °C / Inert atmosphere

2: methanesulfonamide / water; tert-butyl alcohol / 16.5 h / 0 - 20 °C

3: pyridine / dichloromethane / 4 h / 0 - 20 °C

4: potassium carbonate / methanol / 1.5 h / 20 °C

5: lithium aluminium tetrahydride / diethyl ether / 2 h / -40 - 0 °C

6: 1H-imidazole; carbon tetrabromide; triphenylphosphine / dichloromethane / 0.5 h / 0 °C

7: n-butyllithium; sodium hydride / tetrahydrofuran / 1 h / 0 °C

8: 1-methyl-1H-imidazole; triethylamine; lithium chloride / dichloromethane / 3 h / 20 °C

With pyridine; 1H-imidazole; 1-methyl-1H-imidazole; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium aluminium tetrahydride; n-butyllithium; carbon tetrabromide; methanesulfonamide; sodium hydride; potassium carbonate; triethylamine; triphenylphosphine; lithium chloride; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1: Negishi coupling reaction;
DOI:10.1055/s-0031-1290803