6-(N-benzyl-but-3-enylamino)-4-methoxy-5-oximinomethyl-2-pivaloylpyrimidine

Base Information

Chemical Name:6-(N-benzyl-but-3-enylamino)-4-methoxy-5-oximinomethyl-2-pivaloylpyrimidine
CAS No.:177483-61-3
Molecular Formula:C₂₂H₂₉N₅O₃
Molecular Weight:411.504
Hs Code.:

Synonyms:6-(N-benzyl-but-3-enylamino)-4-methoxy-5-oximinomethyl-2-pivaloylpyrimidine

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Chemical Property of 6-(N-benzyl-but-3-enylamino)-4-methoxy-5-oximinomethyl-2-pivaloylpyrimidine

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Technology Process of 6-(N-benzyl-but-3-enylamino)-4-methoxy-5-oximinomethyl-2-pivaloylpyrimidine

There total 4 articles about 6-(N-benzyl-but-3-enylamino)-4-methoxy-5-oximinomethyl-2-pivaloylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 177483-60-2
6-(N-benzyl-but-3-enylamino)-5-formyl-4-methoxy-2-pivaloylpyrimidine

: 177483-61-3
6-(N-benzyl-but-3-enylamino)-4-methoxy-5-oximinomethyl-2-pivaloylpyrimidine

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; for 2h; Ambient temperature;
DOI:10.1016/0040-4020(96)00232-3

Reference yield:

: 17150-62-8
N-benzyl-3-butenylamine

: 177483-61-3
6-(N-benzyl-but-3-enylamino)-4-methoxy-5-oximinomethyl-2-pivaloylpyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / Et₃N / ethanol / 4 h / Heating

2: 94 percent / methanol / 2.5 h / Heating

3: 86 percent / 4-dimethylaminopyridine / toluene / 18 h / Heating

4: 87 percent / hydroxylamine hydrochloride, pyridine / ethanol / 2 h / Ambient temperature

With pyridine; dmap; hydroxylamine hydrochloride; triethylamine; In methanol; ethanol; toluene;
DOI:10.1016/0040-4020(96)00232-3

Reference yield:

: 177483-59-9
2-amino-6-(N-benzyl-but-3-enylamino)-5-formyl-4-methoxypyrimidine

: 177483-61-3
6-(N-benzyl-but-3-enylamino)-4-methoxy-5-oximinomethyl-2-pivaloylpyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / 4-dimethylaminopyridine / toluene / 18 h / Heating

2: 87 percent / hydroxylamine hydrochloride, pyridine / ethanol / 2 h / Ambient temperature

With pyridine; dmap; hydroxylamine hydrochloride; In ethanol; toluene;
DOI:10.1016/0040-4020(96)00232-3