2'-(5'-O-dimethoxytrityl-N₆,N₆,3'-O-tribenzoyladenosyl)-8-(5-chloro-8-quinolyl) phosphate triethylammonium salt

Base Information

• Chemical Name: 2'-(5'-O-dimethoxytrityl-N₆,N₆,3'-O-tribenzoyladenosyl)-8-(5-chloro-8-quinolyl) phosphate triethylammonium salt
• CAS No.: 108257-57-4
• Molecular Formula: C₆H₁₅N*C₆₁H₄₈ClN₆O₁₂P
• Molecular Weight: 1224.7

Synonyms:2'-(5'-O-dimethoxytrityl-N₆,N₆,3'-O-tribenzoyladenosyl)-8-(5-chloro-8-quinolyl) phosphate triethylammonium salt

Chemical Property of 2'-(5'-O-dimethoxytrityl-N₆,N₆,3'-O-tribenzoyladenosyl)-8-(5-chloro-8-quinolyl) phosphate triethylammonium salt

Chemical Property:

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Technology Process of 2'-(5'-O-dimethoxytrityl-N₆,N₆,3'-O-tribenzoyladenosyl)-8-(5-chloro-8-quinolyl) phosphate triethylammonium salt

There total 5 articles about 2'-(5'-O-dimethoxytrityl-N₆,N₆,3'-O-tribenzoyladenosyl)-8-(5-chloro-8-quinolyl) phosphate triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3'-O-benzoyladenosine (42822-84-4) → 2'-(5'-O-dimethoxytrityl-N6,N6,3'-O-tribenzoyladenosyl)-8-(5-chloro-8-quinolyl) phosphate triethylammonium salt (108257-57-4)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridine / 1 h / Ambient temperature

2: pyridine / 4 h

3: 91 percent / pyridine / 1 h

4: 1.) QsCl / 1.) pyridine, 1 h; 2.) CH₂Cl₂, MeOH

With 1.) QsCl; In pyridine;

Reference yield:

4,4'-dimethoxytrityl chloride (40615-36-9) → 2'-(5'-O-dimethoxytrityl-N6,N6,3'-O-tribenzoyladenosyl)-8-(5-chloro-8-quinolyl) phosphate triethylammonium salt (108257-57-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / pyridine / 1 h

2: 1.) QsCl / 1.) pyridine, 1 h; 2.) CH₂Cl₂, MeOH

With 1.) QsCl; In pyridine;

Reference yield:

Benzoic acid (2R,3R,4R,5R)-5-(6-amino-purin-9-yl)-4-trimethylsilanyloxy-2-trimethylsilanyloxymethyl-tetrahydro-furan-3-yl ester (103022-73-7) → 2'-(5'-O-dimethoxytrityl-N6,N6,3'-O-tribenzoyladenosyl)-8-(5-chloro-8-quinolyl) phosphate triethylammonium salt (108257-57-4)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / 4 h

2: 91 percent / pyridine / 1 h

3: 1.) QsCl / 1.) pyridine, 1 h; 2.) CH₂Cl₂, MeOH

With 1.) QsCl; In pyridine;

upstream raw materials:

O-8-(5-chloroquinolyl) phosphate

N₆,N₆,3'-O-tribenzoyl-5'-O-dimethoxytrityladenosine

triethylamine

3'-O-benzoyladenosine

Downstream raw materials:

C₁₃₉H₁₀₃Cl₂N₁₇O₂₈P₂

C₁₃₉H₁₀₂BrCl₂N₁₇O₂₈P₂

C₉₉H₇₄BrClN₁₁O₁₉P

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