C₂₄H₃₀O₆

Base Information

Chemical Name:C₂₄H₃₀O₆
CAS No.:1320210-73-8
Molecular Formula:C₂₄H₃₀O₆
Molecular Weight:414.499
Hs Code.:

C<sub>24</sub>H<sub>30</sub>O<sub>6</sub>

Synonyms:C₂₄H₃₀O₆

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Chemical Property of C₂₄H₃₀O₆

Chemical Property:

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Technology Process of C₂₄H₃₀O₆

There total 7 articles about C₂₄H₃₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1320210-72-7
C₂₄H₂₈O₆

: 1320210-73-8
C₂₄H₃₀O₆

Guidance literature:: C₂₄H₂₈O₆; With sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; toluene; at -40 - 20 ℃; for 6h; Inert atmosphere;

With water; rochelle salt; In tetrahydrofuran; toluene; Saturated solution;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: 131310-61-7
(2R,4aR,6S,7R,8aS)-6-Methyl-2-phenyl-6-vinyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol

: 1320210-73-8
C₂₄H₃₀O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere

2.1: ozone / methanol; dichloromethane / -78 °C

2.2: -78 - 20 °C

3.1: benzene / 2 h / Inert atmosphere; Reflux

4.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

5.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

5.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

6.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

6.2: Saturated solution

With titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; sodium hydride; diisobutylaluminium hydride; ozone; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; benzene; 3.1: Wittig reaction / 5.1: Sharpless epoxidation / 5.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: C₂₃H₂₆O₄

: 1320210-73-8
C₂₄H₃₀O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: ozone / methanol; dichloromethane / -78 °C

1.2: -78 - 20 °C

2.1: benzene / 2 h / Inert atmosphere; Reflux

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

4.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

4.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

5.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

5.2: Saturated solution

With titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; diisobutylaluminium hydride; ozone; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene; benzene; 2.1: Wittig reaction / 4.1: Sharpless epoxidation / 4.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071