9-<(2-hydroxyethoxy)methyl>-N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanine

Base Information

• Chemical Name: 9-<(2-hydroxyethoxy)methyl>-N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanine
• CAS No.: 128060-06-0
• Molecular Formula: C₂₅H₂₅N₇O₉
• Molecular Weight: 567.515

Synonyms:9-<(2-hydroxyethoxy)methyl>-N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanine

Chemical Property of 9-<(2-hydroxyethoxy)methyl>-N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanine

Chemical Property:

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Technology Process of 9-<(2-hydroxyethoxy)methyl>-N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanine

There total 5 articles about 9-<(2-hydroxyethoxy)methyl>-N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

9-<(2-acetoxyethoxy)methyl>-N2-<2-(4-nitrophenyl)ethoxycarbonyl>-O6-<2-(4-nitrophenyl)ethyl>guanine (128060-05-9) → 9-<(2-hydroxyethoxy)methyl>-N2-<2-(4-nitrophenyl)ethoxycarbonyl>-O6-<2-(4-nitrophenyl)ethyl>guanine (128060-06-0)

Guidance literature:

With ammonium hydroxide; In 1,4-dioxane; methanol; at 4 ℃;

DOI:10.1002/hlca.19890720811

Reference yield:

2-(4-nitrophenyl)ethanol (100-27-6) → 9-<(2-hydroxyethoxy)methyl>-N2-<2-(4-nitrophenyl)ethoxycarbonyl>-O6-<2-(4-nitrophenyl)ethyl>guanine (128060-06-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 72 percent / diethyl azodicarboxylate, triphenylphosphine / dioxane / 10 h / Ambient temperature

2: 97 percent / pyridine; CH₂Cl₂ / Ambient temperature

3: 86 percent / 25percent aq. NH₃ / dioxane; methanol / 4 °C

With ammonium hydroxide; triphenylphosphine; diethylazodicarboxylate; In 1,4-dioxane; pyridine; methanol; dichloromethane;

DOI:10.1002/hlca.19890720811

Reference yield:

9-<(2-acetoxyethoxy)methyl>guanine (102728-64-3) → 9-<(2-hydroxyethoxy)methyl>-N2-<2-(4-nitrophenyl)ethoxycarbonyl>-O6-<2-(4-nitrophenyl)ethyl>guanine (128060-06-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 72 percent / diethyl azodicarboxylate, triphenylphosphine / dioxane / 10 h / Ambient temperature

2: 97 percent / pyridine; CH₂Cl₂ / Ambient temperature

3: 86 percent / 25percent aq. NH₃ / dioxane; methanol / 4 °C

With ammonium hydroxide; triphenylphosphine; diethylazodicarboxylate; In 1,4-dioxane; pyridine; methanol; dichloromethane;

DOI:10.1002/hlca.19890720811

upstream raw materials:

9-<(2-acetoxyethoxy)methyl>-N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanine

2-(4-nitrophenyl)ethanol

9-<(2-acetoxyethoxy)methyl>guanine

9-<(2-acetoxyethoxy)methyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanine

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