E-4-methylstyrylsulfonylacetic acid

Base Information

Chemical Name:E-4-methylstyrylsulfonylacetic acid
CAS No.:155782-82-4
Molecular Formula:C₁₁H₁₂O₄S
Molecular Weight:240.28
Hs Code.:

Synonyms:E-4-methylstyrylsulfonylacetic acid

Suppliers and Price of E-4-methylstyrylsulfonylacetic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of E-4-methylstyrylsulfonylacetic acid

Chemical Property:

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Technology Process of E-4-methylstyrylsulfonylacetic acid

There total 3 articles about E-4-methylstyrylsulfonylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 622-97-9,24936-41-2
1-ethenyl-4-methylbenzene

: 155782-82-4
E-4-methylstyrylsulfonylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / dimethylformamide / 0 °C

2: 1.) NaHCO₃, Na₂SO₃ / 1.) 80-90 deg C, 2.) aq. MeOH

With thionyl chloride; sodium hydrogencarbonate; sodium sulfite; In N,N-dimethyl-formamide;

Reference yield:

: 622-97-9,24936-41-2
1-ethenyl-4-methylbenzene

: 155782-82-4
E-4-methylstyrylsulfonylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / SO₂Cl₂ / dimethylformamide / 4 h / 85 - 90 °C

2: 1.) aq. NaHCO₃, aq. Na₂SO₃ / 1.) 80 - 90 deg C, 1 h, 2.) H₂O, reflux, 3 h

With sulfuryl dichloride; sodium hydrogencarbonate; sodium sulfite; In N,N-dimethyl-formamide;

Reference yield:

: 98821-28-4
E-4-Methylstyrylsulfonyl Chloride

: 79-11-8
chloroacetic acid

: 155782-82-4
E-4-methylstyrylsulfonylacetic acid

Guidance literature:: With sodium hydrogencarbonate; sodium sulfite; Yield given. Multistep reaction; 1.) 80 - 90 deg C, 1 h, 2.) H₂O, reflux, 3 h;