methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-5-carboxylate

Base Information

• Chemical Name: methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-5-carboxylate
• CAS No.: 869299-53-6
• Molecular Formula: C₁₅H₁₅N₃O₇
• Molecular Weight: 349.3

Synonyms:methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-5-carboxylate

Chemical Property of methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-5-carboxylate

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Technology Process of methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-5-carboxylate

There total 2 articles about methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitro-2H-pyrazole-3-carboxylic acid methyl ester (138786-86-4) + methyl 4-(2-bromoethoxy)benzoate (56850-91-0) → methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-5-carboxylate (869299-53-6) + methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-3-carboxylate (869299-54-7)

Guidance literature:

With potassium carbonate; In acetone; for 4h; Heating / reflux;

Reference yield:

4-nitro-2H-pyrazole-3-carboxylic acid methyl ester (138786-86-4) + 4-(2-Bromo-ethoxy)-benzoic acid ethyl ester (41386-38-3) → methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-5-carboxylate (869299-53-6) + methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-3-carboxylate (869299-54-7)

Guidance literature:

With potassium carbonate; In acetone; for 4h; Overall yield = 7.42 g; Reflux;

Reference yield:

methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-5-carboxylate (869299-53-6) + methyl 1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-4-nitro-1H-pyrazole-3-carboxylate (869299-54-7) → methyl 4-amino-1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-1H-pyrazole-5-carboxylate (869299-52-5) + methyl 4-amino-1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-1H-pyrazole-3-carboxylate (869299-55-8)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol; at 20 ℃; under 760.051 Torr;

upstream raw materials:

4-nitro-2H-pyrazole-3-carboxylic acid methyl ester

methyl 4-(2-bromoethoxy)benzoate

4-(2-Bromo-ethoxy)-benzoic acid ethyl ester

Downstream raw materials:

methyl 4-amino-1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-1H-pyrazole-5-carboxylate

methyl 4-amino-1-[2-({4-[(methyloxy)carbonyl]phenyl}oxy)ethyl]-1H-pyrazole-3-carboxylate

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