3-[2-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-propynoic acid dimethylamide

Base Information

Chemical Name:3-[2-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-propynoic acid dimethylamide
CAS No.:935521-25-8
Molecular Formula:C₁₈H₂₇NO₂Si
Molecular Weight:317.503
Hs Code.:

3-[2-(<i>tert</i>-butyl-dimethyl-silanyloxymethyl)-phenyl]-propynoic acid dimethylamide

Synonyms:3-[2-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-propynoic acid dimethylamide

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Chemical Property of 3-[2-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-propynoic acid dimethylamide

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Technology Process of 3-[2-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-propynoic acid dimethylamide

There total 1 articles about 3-[2-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-propynoic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 173074-01-6
1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-ethynylbenzene

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 935521-25-8
3-[2-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-propynoic acid dimethylamide

Guidance literature:: 1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-ethynylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -40 ℃; for 0.666667h;

N,N-Dimethylcarbamoyl chloride; In tetrahydrofuran; hexane; at -40 - 20 ℃; for 0.666667h;
DOI:10.1016/j.tet.2007.01.046