3-benzyl-6-benzyloxymethyl-9,12,15-triisopropyl-1,4,7,10,13pentaaza-cyclopentadecane-2,5,8,11,14-pentaone

Base Information

Chemical Name:3-benzyl-6-benzyloxymethyl-9,12,15-triisopropyl-1,4,7,10,13pentaaza-cyclopentadecane-2,5,8,11,14-pentaone
CAS No.:934714-91-7
Molecular Formula:C₃₄H₄₇N₅O₆
Molecular Weight:621.777
Hs Code.:

Synonyms:3-benzyl-6-benzyloxymethyl-9,12,15-triisopropyl-1,4,7,10,13pentaaza-cyclopentadecane-2,5,8,11,14-pentaone

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Chemical Property of 3-benzyl-6-benzyloxymethyl-9,12,15-triisopropyl-1,4,7,10,13pentaaza-cyclopentadecane-2,5,8,11,14-pentaone

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Technology Process of 3-benzyl-6-benzyloxymethyl-9,12,15-triisopropyl-1,4,7,10,13pentaaza-cyclopentadecane-2,5,8,11,14-pentaone

There total 13 articles about 3-benzyl-6-benzyloxymethyl-9,12,15-triisopropyl-1,4,7,10,13pentaaza-cyclopentadecane-2,5,8,11,14-pentaone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 934715-79-4
2-(2-{2-[2-(2-amino-3-methyl-butyrylamino)-3-methyl-butyrylamino]-3-methyl-butyrylamino}-3-benzyloxy-propionylamino)-3-phenyl-propionic acid

: 934714-91-7
3-benzyl-6-benzyloxymethyl-9,12,15-triisopropyl-1,4,7,10,13pentaaza-cyclopentadecane-2,5,8,11,14-pentaone

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo061830j

Reference yield:

: 934715-36-3
2-(3-benzyloxy-2-{2-[2-(2-tert-butoxycarbonylamino-3-methyl-butyrylamino)-3-methyl-butyrylamino]-3-methyl-butyrylamino}-propionylamino)-3-phenyl-propionic acid methyl ester

: 934714-91-7
3-benzyl-6-benzyloxymethyl-9,12,15-triisopropyl-1,4,7,10,13pentaaza-cyclopentadecane-2,5,8,11,14-pentaone

Guidance literature:: Multi-step reaction with 2 steps

1: HCl; anisole / tetrahydrofuran

2: 14 percent / ethyldiisopropylamine; 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium BF₄; 2-(1H-7-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluronium PF₆ / acetonitrile; tetrahydrofuran; CH₂Cl₂

With hydrogenchloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo061830j

Reference yield:

: 934715-35-2
2-[2-(2-amino-3-methyl-butyrylamino)-3-benzyloxy-propionylamino]-3-phenyl-propionic acid methyl ester

: 934714-91-7
3-benzyl-6-benzyloxymethyl-9,12,15-triisopropyl-1,4,7,10,13pentaaza-cyclopentadecane-2,5,8,11,14-pentaone

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / ethyldiisopropylamine; 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium BF₄; 2-(1H-7-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluronium PF₆ / acetonitrile / 20 °C

2: HCl; anisole / tetrahydrofuran

3: 14 percent / ethyldiisopropylamine; 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium BF₄; 2-(1H-7-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluronium PF₆ / acetonitrile; tetrahydrofuran; CH₂Cl₂

With hydrogenchloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo061830j