isobutyl N-methyl-N-[(S)-1-methyl-(2-{1,1-dimethyl-2-[methyl(phenyl)amino]-2-thioxoethyl}amino)-2-oxoethyl]carbamate

Base Information

Chemical Name:isobutyl N-methyl-N-[(S)-1-methyl-(2-{1,1-dimethyl-2-[methyl(phenyl)amino]-2-thioxoethyl}amino)-2-oxoethyl]carbamate
CAS No.:351196-88-8
Molecular Formula:C₂₀H₃₁N₃O₃S
Molecular Weight:393.55
Hs Code.:

Synonyms:isobutyl N-methyl-N-[(S)-1-methyl-(2-{1,1-dimethyl-2-[methyl(phenyl)amino]-2-thioxoethyl}amino)-2-oxoethyl]carbamate

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Chemical Property of isobutyl N-methyl-N-[(S)-1-methyl-(2-{1,1-dimethyl-2-[methyl(phenyl)amino]-2-thioxoethyl}amino)-2-oxoethyl]carbamate

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Technology Process of isobutyl N-methyl-N-[(S)-1-methyl-(2-{1,1-dimethyl-2-[methyl(phenyl)amino]-2-thioxoethyl}amino)-2-oxoethyl]carbamate

There total 2 articles about isobutyl N-methyl-N-[(S)-1-methyl-(2-{1,1-dimethyl-2-[methyl(phenyl)amino]-2-thioxoethyl}amino)-2-oxoethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₂₅NO₆

: 351196-88-8
isobutyl N-methyl-N-[(S)-1-methyl-(2-{1,1-dimethyl-2-[methyl(phenyl)amino]-2-thioxoethyl}amino)-2-oxoethyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂S*H₂O / tetrahydrofuran; dimethylsulfoxide / 1 h / -10 °C

2: CH₂Cl₂ / 20 h / 0 - 25 °C

With sodium sulfide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/1522-2675(20010418)84:4<786::AID-HLCA786>3.0.CO;2-A

Reference yield:

: 75755-40-7
2,2-dimethyl-3-(N-methyl-N-phenylamino)-2H-azirine

: (S)-2-(Isobutoxycarbonyl-methyl-amino)-thiopropionic acid

: 351196-88-8
isobutyl N-methyl-N-[(S)-1-methyl-(2-{1,1-dimethyl-2-[methyl(phenyl)amino]-2-thioxoethyl}amino)-2-oxoethyl]carbamate

Guidance literature:: In dichloromethane; at 0 - 25 ℃; for 20h;
DOI:10.1002/1522-2675(20010418)84:4<786::AID-HLCA786>3.0.CO;2-A

Reference yield: 96.0%

: 351196-88-8
isobutyl N-methyl-N-[(S)-1-methyl-(2-{1,1-dimethyl-2-[methyl(phenyl)amino]-2-thioxoethyl}amino)-2-oxoethyl]carbamate

: isobutyl N-methyl-N-[(S)-1-methyl-(2-{1,1-dimethyl-2-[methyl(phenyl)amino]-2-oxoethyl}amino)-2-thioxorthyl]carbamate

Guidance literature:: isobutyl N-methyl-N-[(S)-1-methyl-(2-{1,1-dimethyl-2-[methyl(phenyl)amino]-2-thioxoethyl}amino)-2-oxoethyl]carbamate; With zinc(II) chloride; In acetic acid; at 25 ℃; for 0.025h;

With hydrogenchloride; zinc(II) chloride; In acetic acid; at 25 ℃; for 0.0166667h;
DOI:10.1002/1522-2675(20010418)84:4<786::AID-HLCA786>3.0.CO;2-A