Technology Process of bis<1-(3,5-di-tert-butylphenyl)-1-methylethyl>diazine
There total 4 articles about bis<1-(3,5-di-tert-butylphenyl)-1-methylethyl>diazine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; iodine pentafluoride;
In
dichloromethane;
at -78 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 27.6 g / 85percent sulfuric acid / 7 h / 50 °C
2: 83 percent / bromine, sodium methoxide / 0.75 h / Heating
3: 95 percent / NaOH / methanol / 4 h / 155 °C
4: 83.7 percent / pyridine, iodine pentafluoride / CH2Cl2 / 1 h / -78 °C
With
pyridine; sodium hydroxide; sulfuric acid; bromine; sodium methylate; iodine pentafluoride;
In
methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 83 percent / bromine, sodium methoxide / 0.75 h / Heating
2: 95 percent / NaOH / methanol / 4 h / 155 °C
3: 83.7 percent / pyridine, iodine pentafluoride / CH2Cl2 / 1 h / -78 °C
With
pyridine; sodium hydroxide; bromine; sodium methylate; iodine pentafluoride;
In
methanol; dichloromethane;
