7-amino-1-(2-methoxy-4-methoxycarbonylbenzyl)-4-oxo-1,4-dihydroquinoline

Base Information

Chemical Name:7-amino-1-(2-methoxy-4-methoxycarbonylbenzyl)-4-oxo-1,4-dihydroquinoline
CAS No.:188244-60-2
Molecular Formula:C₁₉H₁₈N₂O₄
Molecular Weight:338.363
Hs Code.:

Synonyms:7-amino-1-(2-methoxy-4-methoxycarbonylbenzyl)-4-oxo-1,4-dihydroquinoline

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Chemical Property of 7-amino-1-(2-methoxy-4-methoxycarbonylbenzyl)-4-oxo-1,4-dihydroquinoline

Chemical Property:

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Technology Process of 7-amino-1-(2-methoxy-4-methoxycarbonylbenzyl)-4-oxo-1,4-dihydroquinoline

There total 5 articles about 7-amino-1-(2-methoxy-4-methoxycarbonylbenzyl)-4-oxo-1,4-dihydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 188244-56-6
1-(2-methoxy-4-methoxycarbonylbenzyl)-7-nitro-4-oxo-1,4-dihydroquinoline

: 188244-60-2
7-amino-1-(2-methoxy-4-methoxycarbonylbenzyl)-4-oxo-1,4-dihydroquinoline

Guidance literature:: With ammonium formate; palladium on activated charcoal; In methanol; for 2.5h; Heating;
DOI:10.1016/S0223-5234(97)83282-5

Reference yield:

: 3556-83-0
methyl 4-methyl-3-methoxybenzoate

: 188244-60-2
7-amino-1-(2-methoxy-4-methoxycarbonylbenzyl)-4-oxo-1,4-dihydroquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NBS, AIBN / CCl₄ / 4 h / Heating

2: 2.) NaH / 1.) diphenyl ether, reflux, 20 min, 2.) THF, 0 deg C, 30 min, 3.) reflux, 4 h

3: 92 percent / ammonium formate / 10percent Pd-C / methanol / 2.5 h / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); ammonium formate; sodium hydride; palladium on activated charcoal; In methanol; tetrachloromethane;
DOI:10.1016/S0223-5234(97)83282-5

Reference yield:

: 70264-94-7
methyl 4-(bromomethyl)-3-methoxybenzoate

: 188244-60-2
7-amino-1-(2-methoxy-4-methoxycarbonylbenzyl)-4-oxo-1,4-dihydroquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) NaH / 1.) diphenyl ether, reflux, 20 min, 2.) THF, 0 deg C, 30 min, 3.) reflux, 4 h

2: 92 percent / ammonium formate / 10percent Pd-C / methanol / 2.5 h / Heating

With ammonium formate; sodium hydride; palladium on activated charcoal; In methanol;
DOI:10.1016/S0223-5234(97)83282-5