Technology Process of triisopropyl(3-phenylanthracen-2-yloxy)silane
There total 4 articles about triisopropyl(3-phenylanthracen-2-yloxy)silane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
[2,2]bipyridinyl; silver(I) triflimide;
In
dichloromethane;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1021/ja302537j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: hydrazine hydrate / ethanol; dichloromethane / 0 - 20 °C / Inert atmosphere
3.1: [2,2]bipyridinyl; silver(I) triflimide / dichloromethane / 3 h / 20 °C / Inert atmosphere
With
[2,2]bipyridinyl; oxalyl dichloride; hydrazine hydrate; dimethyl sulfoxide; silver(I) triflimide;
In
ethanol; dichloromethane;
1.1: Swern oxidation / 1.2: Swern oxidation / 3.1: Diels-Alder reaction;
DOI:10.1021/ja302537j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine hydrate / ethanol; dichloromethane / 0 - 20 °C / Inert atmosphere
2: [2,2]bipyridinyl; silver(I) triflimide / dichloromethane / 3 h / 20 °C / Inert atmosphere
With
[2,2]bipyridinyl; hydrazine hydrate; silver(I) triflimide;
In
ethanol; dichloromethane;
2: Diels-Alder reaction;
DOI:10.1021/ja302537j
