C₃₃H₃₃IO₆

Base Information

Chemical Name:C₃₃H₃₃IO₆
CAS No.:1571073-02-3
Molecular Formula:C₃₃H₃₃IO₆
Molecular Weight:652.526
Hs Code.:

C<sub>33</sub>H<sub>33</sub>IO<sub>6</sub>

Synonyms:C₃₃H₃₃IO₆

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Chemical Property of C₃₃H₃₃IO₆

Chemical Property:

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Technology Process of C₃₃H₃₃IO₆

There total 6 articles about C₃₃H₃₃IO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1428631-86-0
C₁₂H₁₅IO₄

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1571073-02-3
C₃₃H₃₃IO₆

Guidance literature:: With pyridine; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jo4028227

Reference yield:

: 173327-56-5
3,5-bis-O,O-(tert-butyldimethylsilyl)-1,2-didehydro-1,2-dideoxy-D-ribofuranose

: 1571073-02-3
C₃₃H₃₃IO₆

Guidance literature:: Multi-step reaction with 5 steps

1: tributyl-amine; palladium diacetate; triphenyl-arsane / N,N-dimethyl-formamide / 15 h / 70 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / N,N-dimethyl-formamide; tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

3: sodium tris(acetoxy)borohydride / acetic acid; acetonitrile / 1 h / 0 °C / Inert atmosphere

4: sodium iodide; N,N’-trans-dimethyl cyclohexane-1,2-diamine / pentan-1-ol / 3 h / 130 °C / Inert atmosphere

5: pyridine / 16 h / 20 °C / Inert atmosphere

With pyridine; tributyl-amine; triphenyl-arsane; tetrabutyl ammonium fluoride; palladium diacetate; sodium tris(acetoxy)borohydride; sodium iodide; N,N’-trans-dimethyl cyclohexane-1,2-diamine; In tetrahydrofuran; pentan-1-ol; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo4028227

Reference yield:

: 1571073-00-1
C₁₂H₁₃BrO₄

: 1571073-02-3
C₃₃H₃₃IO₆

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / acetic acid; acetonitrile / 1 h / 0 °C / Inert atmosphere

2: sodium iodide; N,N’-trans-dimethyl cyclohexane-1,2-diamine / pentan-1-ol / 3 h / 130 °C / Inert atmosphere

3: pyridine / 16 h / 20 °C / Inert atmosphere

With pyridine; sodium tris(acetoxy)borohydride; sodium iodide; N,N’-trans-dimethyl cyclohexane-1,2-diamine; In pentan-1-ol; acetic acid; acetonitrile;
DOI:10.1021/jo4028227