8-C-β-D-glucopyranosylorobol

Base Information

Chemical Name:8-C-β-D-glucopyranosylorobol
CAS No.:66026-81-1
Molecular Formula:C₂₁H₂₀O₁₁
Molecular Weight:448.383
Hs Code.:

Synonyms:8-C-β-D-glucopyranosylorobol

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Chemical Property of 8-C-β-D-glucopyranosylorobol

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 8-C-β-D-glucopyranosylorobol

There total 3 articles about 8-C-β-D-glucopyranosylorobol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 898550-58-8
2'-acetoxy-3,4,4',6'-tetra(benzyloxy)-3'-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)chalcone

: 66026-81-1
8-C-β-D-glucopyranosylorobol

Guidance literature:: 2'-acetoxy-3,4,4',6'-tetra(benzyloxy)-3'-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)chalcone; With thallium(III) nitrate; In methanol; at 40 ℃; for 23h;

With hydrogenchloride; In 1,4-dioxane; methanol; for 22h; Heating;

With hydrogen; palladium dihydroxide; In methanol; ethyl acetate; at 20 ℃; for 5h;
DOI:10.1016/j.carres.2006.03.038

Reference yield:

: 169566-46-5
1-(4,6-bis(benzyloxy)-2-hydroxy-3-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)phenyl)ethanone

: 66026-81-1
8-C-β-D-glucopyranosylorobol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / NaOMe / dioxane; methanol / 20 h / 20 °C

2.1: 90 percent / DMAP; pyridine / 20 h / 20 °C

3.1: thallium(III) nitrate / methanol; various solvent(s) / 23 h / 40 °C

3.2: aq. HCl / dioxane; methanol / 22 h / Heating

3.3: 88.6 mg / hydrogen / Pd(OH)2/C / methanol; ethyl acetate / 5 h / 20 °C

With pyridine; dmap; sodium methylate; thallium(III) nitrate; In 1,4-dioxane; methanol;
DOI:10.1016/j.carres.2006.03.038

Reference yield:

: 381686-06-2
3,4,4',6'-tetrakis-benzyloxy-3'-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2'-hydroxychalcone

: 66026-81-1
8-C-β-D-glucopyranosylorobol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 90 percent / DMAP; pyridine / 20 h / 20 °C

2.1: thallium(III) nitrate / methanol; various solvent(s) / 23 h / 40 °C

2.2: aq. HCl / dioxane; methanol / 22 h / Heating

2.3: 88.6 mg / hydrogen / Pd(OH)2/C / methanol; ethyl acetate / 5 h / 20 °C

With pyridine; dmap; thallium(III) nitrate; In methanol;
DOI:10.1016/j.carres.2006.03.038