8bH-3,4-dihydro-1-(4-methylphenyl)-diazirino<3,1-a>isochinolin

Base Information

• Chemical Name: 8bH-3,4-dihydro-1-(4-methylphenyl)-diazirino<3,1-a>isochinolin
• CAS No.: 77896-82-3
• Molecular Formula: C₁₆H₁₆N₂
• Molecular Weight: 236.316
• Mol file: 77896-82-3.mol

Synonyms:8bH-3,4-dihydro-1-(4-methylphenyl)-diazirino<3,1-a>isochinolin

Chemical Property of 8bH-3,4-dihydro-1-(4-methylphenyl)-diazirino<3,1-a>isochinolin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 8bH-3,4-dihydro-1-(4-methylphenyl)-diazirino<3,1-a>isochinolin

There total 2 articles about 8bH-3,4-dihydro-1-(4-methylphenyl)-diazirino<3,1-a>isochinolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

5,6,8a,13,14,16a-hexahydro-8,16-di-(4-methylphenyl)-s-tetrazino<6,1-a:3,4-a'>diisochinolin (77896-81-2) → 8bH-3,4-dihydro-1-(4-methylphenyl)-diazirino<3,1-a>isochinolin (77896-82-3)

Guidance literature:

In cyclohexane; at 65 ℃; Irradiation;

DOI:10.1016/S0040-4039(00)71143-9

Reference yield:

3,4,-dihydro-isochinolinium-2-(4-methylphenylimid) (77910-08-8) → 8bH-3,4-dihydro-1-(4-methylphenyl)-diazirino<3,1-a>isochinolin (77896-82-3)

Guidance literature:

In cyclohexane; at 65 ℃; Product distribution; Irradiation; photolysis and valence tautomerism;

DOI:10.1016/S0040-4039(00)71143-9

Reference yield:

8bH-3,4-dihydro-1-(4-methylphenyl)-diazirino<3,1-a>isochinolin (77896-82-3) → 5,6,8a,13,14,16a-hexahydro-8,16-di-(4-methylphenyl)-s-tetrazino<6,1-a:3,4-a'>diisochinolin (77896-81-2)

Guidance literature:

In cyclohexane; Product distribution; Heating; valence tautomerism;

DOI:10.1016/S0040-4039(00)71143-9

upstream raw materials:

3,4,-dihydro-isochinolinium-2-(4-methylphenylimid)

5,6,8a,13,14,16a-hexahydro-8,16-di-(4-methylphenyl)-s-tetrazino<6,1-a:3,4-a'>diisochinolin

Downstream raw materials:

5,6,8a,13,14,16a-hexahydro-8,16-di-(4-methylphenyl)-s-tetrazino<6,1-a:3,4-a'>diisochinolin