Technology Process of C66H104N4O12S2
There total 9 articles about C66H104N4O12S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C33H54N2O5S; C33H52N2O8S;
In
acetic anhydride;
at 20 ℃;
With
trifluoroacetic acid;
In
acetic anhydride;
at 20 ℃;
for 3h;
Cooling with ice;
With
pyridine; sodium hydrogencarbonate;
In
water; acetic anhydride;
at 20 ℃;
for 3h;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: bromine; hydrogen bromide / water; methanol / 3.5 h / 30 - 34 °C
2.1: water; ISOPROPYLAMIDE / 4 h / 20 °C
3.1: methanol / Inert atmosphere
3.2: 8 h / 20 °C / Reflux
4.1: ISOPROPYLAMIDE / 3 h / 20 °C
5.1: 1-methyl-pyrrolidin-2-one / 20 °C
5.2: 2 h / 20 °C
6.1: nitrobenzene / ISOPROPYLAMIDE / 2 h / 20 °C
7.1: acetic anhydride / 20 °C
7.2: 3 h / 20 °C / Cooling with ice
7.3: 3 h / 20 °C
With
hydrogen bromide; bromine; nitrobenzene;
In
1-methyl-pyrrolidin-2-one; methanol; ISOPROPYLAMIDE; water; acetic anhydride;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: methanol / Inert atmosphere
1.2: 8 h / 20 °C / Reflux
2.1: ISOPROPYLAMIDE / 3 h / 20 °C
3.1: 1-methyl-pyrrolidin-2-one / 20 °C
3.2: 2 h / 20 °C
4.1: nitrobenzene / ISOPROPYLAMIDE / 2 h / 20 °C
5.1: acetic anhydride / 20 °C
5.2: 3 h / 20 °C / Cooling with ice
5.3: 3 h / 20 °C
With
nitrobenzene;
In
1-methyl-pyrrolidin-2-one; methanol; ISOPROPYLAMIDE; acetic anhydride;