fac-(CH₂CHCH₂CH₂PH₂)3molybdenum(CO)3

Base Information

• Chemical Name: fac-(CH₂CHCH₂CH₂PH₂)3molybdenum(CO)3
• CAS No.: 121393-42-8
• Molecular Formula: C₁₅H₂₇MoO₃P₃
• Molecular Weight: 444.239
• Mol file: 121393-42-8.mol

Synonyms:fac-(CH₂CHCH₂CH₂PH₂)3molybdenum(CO)3

Chemical Property of fac-(CH₂CHCH₂CH₂PH₂)3molybdenum(CO)3

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of fac-(CH₂CHCH₂CH₂PH₂)3molybdenum(CO)3

There total 2 articles about fac-(CH₂CHCH₂CH₂PH₂)3molybdenum(CO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tricarbonylmesitylenemolybdenum(0) (12089-15-5) + CH2CHCH2CH2PH2 (114596-01-9) → fac-(CH2CHCH2CH2PH2)3molybdenum(CO)3 (121393-42-8) + 1,3,5-trimethyl-benzene (108-67-8)

Guidance literature:

In benzene; React. of 3 equiv of org. compd. with stirred suspn. of Mo-complex in benzene (25°C, inert-atmosphere).; Removal of benzene, unreacted phosphine and mes after 48 h in vac., dissolving of resulting materials in benzene and passing of soln. through alumina column. Removal of benzene (vac.) gives pure complex as viscous oil.;

Reference yield:

tricarbonyl(cycloheptatriene)molybdenum(0) (121719-12-8,12125-77-8) + CH2CHCH2CH2PH2 (114596-01-9) → fac-(CH2CHCH2CH2PH2)3molybdenum(CO)3 (121393-42-8) + Cyclohepta-1,3,5-triene (544-25-2)

Guidance literature:

In toluene; React. of 3 equiv of org. compd. with Mo-complex in toluene (25°C, inert-atmosphere).; Removal of solvent and cycloheptatriene in vac. gives pure complex.;

upstream raw materials:

tricarbonyl(cycloheptatriene)molybdenum⁽⁰⁾

CH₂CHCH₂CH₂PH₂

tricarbonylmesitylenemolybdenum⁽⁰⁾

Refernces