ethyl 3-[4-(4-N,N-dimethylaminobenzoyl)-1-methyl-1H-2-pyrrolyl]-2-propenoate

Base Information

Chemical Name:ethyl 3-[4-(4-N,N-dimethylaminobenzoyl)-1-methyl-1H-2-pyrrolyl]-2-propenoate
CAS No.:128843-43-6
Molecular Formula:C₁₉H₂₂N₂O₃
Molecular Weight:326.395
Hs Code.:

Synonyms:ethyl 3-[4-(4-N,N-dimethylaminobenzoyl)-1-methyl-1H-2-pyrrolyl]-2-propenoate

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Chemical Property of ethyl 3-[4-(4-N,N-dimethylaminobenzoyl)-1-methyl-1H-2-pyrrolyl]-2-propenoate

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Technology Process of ethyl 3-[4-(4-N,N-dimethylaminobenzoyl)-1-methyl-1H-2-pyrrolyl]-2-propenoate

There total 4 articles about ethyl 3-[4-(4-N,N-dimethylaminobenzoyl)-1-methyl-1H-2-pyrrolyl]-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 128843-63-0
4-<4-(dimethylamino)benzoyl>-1-methyl-1H-pyrrole-2-carboxaldehyde

: 128843-43-6
ethyl 3-[4-(4-N,N-dimethylaminobenzoyl)-1-methyl-1H-2-pyrrolyl]-2-propenoate

Guidance literature:: With potassium carbonate; In ethanol;
DOI:10.1021/jm00172a026

Reference yield:

: 96-54-8
N-Methylpyrrole

: 128843-43-6
ethyl 3-[4-(4-N,N-dimethylaminobenzoyl)-1-methyl-1H-2-pyrrolyl]-2-propenoate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride / 1,2-dichloro-ethane / 0.25 h / 20 °C

2: AlCl₃ / 1,2-dichloro-ethane / 3 h

3: K₂CO₃ / ethanol / 2 h / 70 °C

With aluminium trichloride; oxalyl dichloride; potassium carbonate; In ethanol; 1,2-dichloro-ethane; 1: Vilsmeier-Haack reaction / 2: Friedel-Crafts reaction / 3: Wittig-Horner reaction;
DOI:10.1021/jm021070e

Reference yield:

: 1192-58-1
N-methylpyrrole aldehyde

: 128843-43-6
ethyl 3-[4-(4-N,N-dimethylaminobenzoyl)-1-methyl-1H-2-pyrrolyl]-2-propenoate

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / 1,2-dichloro-ethane / 3 h

2: K₂CO₃ / ethanol / 2 h / 70 °C

With aluminium trichloride; potassium carbonate; In ethanol; 1,2-dichloro-ethane; 1: Friedel-Crafts reaction / 2: Wittig-Horner reaction;
DOI:10.1021/jm021070e