C₃₅H₅₃N₃O₇

Base Information

Chemical Name:C₃₅H₅₃N₃O₇
CAS No.:1255213-63-8
Molecular Formula:C₃₅H₅₃N₃O₇
Molecular Weight:627.822
Hs Code.:

C<sub>35</sub>H<sub>53</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:C₃₅H₅₃N₃O₇

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Chemical Property of C₃₅H₅₃N₃O₇

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Technology Process of C₃₅H₅₃N₃O₇

There total 18 articles about C₃₅H₅₃N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1255213-55-8
C₃₅H₄₉N₃O₉

: 1255213-63-8
C₃₅H₅₃N₃O₇

Guidance literature:: With 20% palladium hydroxide on carbon; hydrogen; In methanol; at 20 ℃;
DOI:10.1021/ja105119r

Reference yield:

: 1255213-20-7
(R)-methyl 5-nitro-2-(pent-4-en-2-yloxy)benzoate

: 1255213-63-8
C₃₅H₅₃N₃O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: water; sodium hydroxide / tetrahydrofuran; methanol / 23 h

1.2: pH 1

2.1: thionyl chloride / 2 h / 85 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 0 - 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 14 h / 0 - 20 °C

6.1: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / toluene / 14 h / 23 °C / Inert atmosphere

7.1: 20% palladium hydroxide on carbon; hydrogen / methanol / 20 °C

With thionyl chloride; Hoveyda-Grubbs catalyst second generation; 20% palladium hydroxide on carbon; tetrabutyl ammonium fluoride; water; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; p-benzoquinone; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ja105119r

Reference yield:

: 1255214-43-7
(R)-5-nitro-2-(pent-4-en-2-yloxy)benzoic acid

: 1255213-63-8
C₃₅H₅₃N₃O₇

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / 2 h / 85 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 0 - 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C

4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 14 h / 0 - 20 °C

5: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / toluene / 14 h / 23 °C / Inert atmosphere

6: 20% palladium hydroxide on carbon; hydrogen / methanol / 20 °C

With thionyl chloride; Hoveyda-Grubbs catalyst second generation; 20% palladium hydroxide on carbon; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ja105119r