Technology Process of 1,3-dihydroxy-2-methyl-5-nonadecylbenzene
There total 3 articles about 1,3-dihydroxy-2-methyl-5-nonadecylbenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron tribromide;
In
dichloromethane;
at 0 - 20 ℃;
for 6.5h;
Inert atmosphere;
DOI:10.1002/cbdv.201600255
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N,N-dimethyl-formamide; oxalyl dichloride / toluene / 3.67 h / 0 - 20 °C
2: Bis<2-(N,N-dimethylamino)aethyl>aether / tetrahydrofuran / 5.33 h / -78 - 20 °C / Inert atmosphere
3: potassium hydroxide; hydrazine hydrate / 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; water / 3 h / 200 °C / Inert atmosphere
4: boron tribromide / dichloromethane / 6.5 h / 0 - 20 °C / Inert atmosphere
With
oxalyl dichloride; Bis<2-(N,N-dimethylamino)aethyl>aether; boron tribromide; hydrazine hydrate; N,N-dimethyl-formamide; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; water; toluene; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol;
DOI:10.1002/cbdv.201600255
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Bis<2-(N,N-dimethylamino)aethyl>aether / tetrahydrofuran / 5.33 h / -78 - 20 °C / Inert atmosphere
2: potassium hydroxide; hydrazine hydrate / 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; water / 3 h / 200 °C / Inert atmosphere
3: boron tribromide / dichloromethane / 6.5 h / 0 - 20 °C / Inert atmosphere
With
Bis<2-(N,N-dimethylamino)aethyl>aether; boron tribromide; hydrazine hydrate; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; water; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol;
DOI:10.1002/cbdv.201600255
