methyl onate 4-phosphate

Base Information

Chemical Name:methyl onate 4-phosphate
CAS No.:135195-75-4
Molecular Formula:C₅₆H₅₇Cl₆O₂₀P
Molecular Weight:1293.75
Hs Code.:

methyl <allyl 7,8-O-cyclohexylidene-3-deoxy-5-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-manno-oct-2-ulopyranosid>onate 4-<bis(trichloroethyl)>phosphate

Synonyms:methyl onate 4-phosphate

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Chemical Property of methyl onate 4-phosphate

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Technology Process of methyl onate 4-phosphate

There total 10 articles about methyl onate 4-phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 17672-53-6
bis-(2,2,2-trichloroethyl)phosphorochloridate

: 135195-73-2
methyl onate

: 135195-75-4
methyl onate 4-phosphate

Guidance literature:: With 1-methyl-1H-imidazole; In tetrahydrofuran; at 40 ℃; for 1h;

Reference yield:

: 14218-11-2,14218-30-5,61198-88-7,108438-33-1,108836-02-8,114682-36-9,127305-34-4,151377-77-4
2,3,4,6-Tetra-O-benzoyl-α-D-mannopyranosyl bromide

: 135195-75-4
methyl onate 4-phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 70.5 percent / N,N,N',N'-tetramethylurea, silver trifluoromethylsulphonate / 1,2-dichloro-ethane / 40 °C

2: 94 percent / Bu₄NF / tetrahydrofuran / 1 h / Ambient temperature

3: 91 percent / N-methylimidazole / tetrahydrofuran / 1 h / 40 °C

With 1-methyl-1H-imidazole; tetrabutyl ammonium fluoride; silver trifluoromethanesulfonate; tetramethylurea; In tetrahydrofuran; 1,2-dichloro-ethane;

Reference yield:

: 931-57-7
1-methoxy-cyclohex-1-ene

: 135195-75-4
methyl onate 4-phosphate

Guidance literature:: Multi-step reaction with 6 steps

1: 61 percent / CuSO₄, p-TsOH / dioxane / Ambient temperature

2: 1) Bu₂SnO, 2) Bu₄NBr / 1) toluene, 2h, reflux, 2) 17h, reflux

3: 65 percent / methanol; CHCl₃ / 2 h / Ambient temperature

4: 70.5 percent / N,N,N',N'-tetramethylurea, silver trifluoromethylsulphonate / 1,2-dichloro-ethane / 40 °C

5: 94 percent / Bu₄NF / tetrahydrofuran / 1 h / Ambient temperature

6: 91 percent / N-methylimidazole / tetrahydrofuran / 1 h / 40 °C

With 1-methyl-1H-imidazole; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; silver trifluoromethanesulfonate; di(n-butyl)tin oxide; toluene-4-sulfonic acid; copper(II) sulfate; tetramethylurea; In tetrahydrofuran; 1,4-dioxane; methanol; chloroform; 1,2-dichloro-ethane;