(4'R,5'R)-4-benzyloxy-2-(4',5'-dimethyl-1',3'-dioxolan-2'-yl)-1-methoxyanthraquinone

Base Information

Chemical Name:(4'R,5'R)-4-benzyloxy-2-(4',5'-dimethyl-1',3'-dioxolan-2'-yl)-1-methoxyanthraquinone
CAS No.:130514-62-4
Molecular Formula:C₂₇H₂₄O₆
Molecular Weight:444.484
Hs Code.:

Synonyms:(4'R,5'R)-4-benzyloxy-2-(4',5'-dimethyl-1',3'-dioxolan-2'-yl)-1-methoxyanthraquinone

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Chemical Property of (4'R,5'R)-4-benzyloxy-2-(4',5'-dimethyl-1',3'-dioxolan-2'-yl)-1-methoxyanthraquinone

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Technology Process of (4'R,5'R)-4-benzyloxy-2-(4',5'-dimethyl-1',3'-dioxolan-2'-yl)-1-methoxyanthraquinone

There total 13 articles about (4'R,5'R)-4-benzyloxy-2-(4',5'-dimethyl-1',3'-dioxolan-2'-yl)-1-methoxyanthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 130514-59-9
(4'R,5'R)-4-benzyloxy-2-(4',5'-dimethyl-1',3'-dioxolan-2'-yl)-1-hydroxyanthraquinone

: 77-78-1
dimethyl sulfate

: 130514-62-4
(4'R,5'R)-4-benzyloxy-2-(4',5'-dimethyl-1',3'-dioxolan-2'-yl)-1-methoxyanthraquinone

Guidance literature:: With potassium carbonate; In acetone; for 12h; Heating;

Reference yield: 98.0%

: 24347-58-8
(R,R)-2,3-butandiol

: 163151-50-6
4-benzyloxy-1-methoxy-9,10-dioxo-9,10-dihydroanthracene-2-carbaldehyde

: 130514-62-4
(4'R,5'R)-4-benzyloxy-2-(4',5'-dimethyl-1',3'-dioxolan-2'-yl)-1-methoxyanthraquinone

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; for 19h; Ambient temperature;

Reference yield:

: 86842-00-4
5-Hydroxy-2-methyl-anthra[1,2-b]furan-6,11-dione

: 130514-62-4
(4'R,5'R)-4-benzyloxy-2-(4',5'-dimethyl-1',3'-dioxolan-2'-yl)-1-methoxyanthraquinone

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / potassium iodide, potassium carbonate / acetone / 96 h / Heating

2: 1.) ozone, 2.) dimethyl sulfide / 1.) dichloromethane, -78 deg C, 1 h, 2.) from -78 deg C to -20 deg C, 1 h

3: aq. sodium hydrogencarbonate / 1 h

4: 66 percent / p-toluenesulfonic acid / benzene / 2 h / Heating

5: 100 percent / potassium carbonate / acetone / 12 h / Heating

With dimethylsulfide; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; ozone; potassium iodide; In acetone; benzene;