2-(4-methylbenzoylamino)-3-hydroperoxy-2,3,4,5,6,7-hexahydro-1,2-benzisothiazole 1,1-dioxide

Base Information

• Chemical Name: 2-(4-methylbenzoylamino)-3-hydroperoxy-2,3,4,5,6,7-hexahydro-1,2-benzisothiazole 1,1-dioxide
• CAS No.: 274692-46-5
• Molecular Formula: C₁₅H₁₈N₂O₅S
• Molecular Weight: 338.384

Synonyms:2-(4-methylbenzoylamino)-3-hydroperoxy-2,3,4,5,6,7-hexahydro-1,2-benzisothiazole 1,1-dioxide

Chemical Property of 2-(4-methylbenzoylamino)-3-hydroperoxy-2,3,4,5,6,7-hexahydro-1,2-benzisothiazole 1,1-dioxide

Chemical Property:

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Technology Process of 2-(4-methylbenzoylamino)-3-hydroperoxy-2,3,4,5,6,7-hexahydro-1,2-benzisothiazole 1,1-dioxide

There total 1 articles about 2-(4-methylbenzoylamino)-3-hydroperoxy-2,3,4,5,6,7-hexahydro-1,2-benzisothiazole 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

C15H16N2OS (148953-47-3) → 2-(4-methylbenzoylamino)-4,5,6,7-tetrahydro-1,2-benzisothiazol-3(2H)-one 1,1-dioxide + 2-(4-methylbenzoylamino)-3-hydroperoxy-2,3,4,5,6,7-hexahydro-1,2-benzisothiazole 1,1-dioxide (274692-46-5)

Guidance literature:

With dihydrogen peroxide; In acetic acid; at 20 ℃; for 8h;

Reference yield: 76.0%

2-(4-methylbenzoylamino)-3-hydroperoxy-2,3,4,5,6,7-hexahydro-1,2-benzisothiazole 1,1-dioxide (274692-46-5) → 3-hydroxy-2-(4-methylbenzoylamino)-2,3,4,5,6,7-hexahydro-1,2-benzisothiazole 1,1-dioxide (274692-58-9)

Guidance literature:

With sodium sulfite; In water; at 20 ℃; for 8h;

Reference yield: 20.0%

2-(4-methylbenzoylamino)-3-hydroperoxy-2,3,4,5,6,7-hexahydro-1,2-benzisothiazole 1,1-dioxide (274692-46-5) → 2-(4-methylbenzoylamino)-4,5,6,7-tetrahydro-1,2-benzisothiazol-3(2H)-one 1,1-dioxide

Guidance literature:

In ethanol; for 2h; Heating;

upstream raw materials:

C₁₅H₁₆N₂OS

Downstream raw materials:

3-hydroxy-2-(4-methylbenzoylamino)-2,3,4,5,6,7-hexahydro-1,2-benzisothiazole 1,1-dioxide

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