(+)-(2S,3S)-benzyl 2-(2-oxopropyl)-3-(triisopropylsilyloxy)piperidine-1-carboxylate

Base Information

Chemical Name:(+)-(2S,3S)-benzyl 2-(2-oxopropyl)-3-(triisopropylsilyloxy)piperidine-1-carboxylate
CAS No.:1186292-59-0
Molecular Formula:C₂₅H₄₁NO₄Si
Molecular Weight:447.69
Hs Code.:

Synonyms:(+)-(2S,3S)-benzyl 2-(2-oxopropyl)-3-(triisopropylsilyloxy)piperidine-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(2S,3S)-benzyl 2-(2-oxopropyl)-3-(triisopropylsilyloxy)piperidine-1-carboxylate

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Technology Process of (+)-(2S,3S)-benzyl 2-(2-oxopropyl)-3-(triisopropylsilyloxy)piperidine-1-carboxylate

There total 1 articles about (+)-(2S,3S)-benzyl 2-(2-oxopropyl)-3-(triisopropylsilyloxy)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 13154-24-0
triisopropylsilyl chloride

: 1186292-58-9
(+)-(3aS,7aS)-benzyl 2-hydroxy-2-methylhexahydrofuro[3,2-b]pyridine-4(2H)-carboxylate

: 1186292-59-0
(+)-(2S,3S)-benzyl 2-(2-oxopropyl)-3-(triisopropylsilyloxy)piperidine-1-carboxylate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja9056322

Reference yield:

: 1186292-59-0
(+)-(2S,3S)-benzyl 2-(2-oxopropyl)-3-(triisopropylsilyloxy)piperidine-1-carboxylate

: C₂₅H₄₀BrNO₄Si

Guidance literature:: (+)-(2S,3S)-benzyl 2-(2-oxopropyl)-3-(triisopropylsilyloxy)piperidine-1-carboxylate; With trimethylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; at 20 ℃; for 0.333333h; Inert atmosphere;

With N-Bromosuccinimide; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja9056322