10-(1,3-dioxolan-2-yl)-1-phenyl-1,7-decadiyne

Base Information

• Chemical Name: 10-(1,3-dioxolan-2-yl)-1-phenyl-1,7-decadiyne
• CAS No.: 1125706-83-3
• Molecular Formula: C₁₉H₂₂O₂
• Molecular Weight: 282.382
• Mol file: 1125706-83-3.mol

Synonyms:10-(1,3-dioxolan-2-yl)-1-phenyl-1,7-decadiyne

Chemical Property of 10-(1,3-dioxolan-2-yl)-1-phenyl-1,7-decadiyne

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of 10-(1,3-dioxolan-2-yl)-1-phenyl-1,7-decadiyne

There total 1 articles about 10-(1,3-dioxolan-2-yl)-1-phenyl-1,7-decadiyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

iodobenzene (591-50-4) + 2-(3,9-decadiynyl)-1,3-dioxolane (87226-59-3) → 10-(1,3-dioxolan-2-yl)-1-phenyl-1,7-decadiyne (1125706-83-3)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; at 40 ℃; for 14h;

DOI:10.1002/ejoc.200800826

Reference yield: 70.0%

10-(1,3-dioxolan-2-yl)-1-phenyl-1,7-decadiyne (1125706-83-3) + 2-bromoallyl bromide (513-31-5) → 2-bromo-14-phenyltetradec-1-ene-7,13-diyn-4-ol (1125707-04-1)

Guidance literature:

With tin; water; hydrogen bromide; In diethyl ether; at 20 ℃; for 120h;

DOI:10.1002/ejoc.200800826

upstream raw materials:

iodobenzene

2-(3,9-decadiynyl)-1,3-dioxolane

Downstream raw materials:

2-bromo-14-phenyltetradec-1-ene-7,13-diyn-4-ol