Technology Process of C27H29N7O3S
There total 8 articles about C27H29N7O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen bromide;
In
acetic acid;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 60 °C
2.1: acetic acid; iron / 2 h / 60 °C
3.1: bromine; acetic acid / 0 - 20 °C
4.1: ethanol / Reflux
5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C
5.2: 0.5 h / 20 °C
6.1: acetic acid; iron / 2 h / 60 °C
7.1: toluene; chloroform / 2 h / 80 °C
8.1: hydrogen bromide / acetic acid / 3 h / 20 °C
With
hydrogen bromide; bromine; iron; sodium hydride; potassium carbonate; acetic acid;
In
ethanol; chloroform; acetic acid; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: acetic acid; iron / 2 h / 60 °C
2.1: bromine; acetic acid / 0 - 20 °C
3.1: ethanol / Reflux
4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C
4.2: 0.5 h / 20 °C
5.1: acetic acid; iron / 2 h / 60 °C
6.1: toluene; chloroform / 2 h / 80 °C
7.1: hydrogen bromide / acetic acid / 3 h / 20 °C
With
hydrogen bromide; bromine; iron; sodium hydride; acetic acid;
In
ethanol; chloroform; acetic acid; N,N-dimethyl-formamide; toluene;