ethyl fluoro-2-(3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosid-2-ulosyl)acetate

Base Information

Chemical Name:ethyl fluoro-2-(3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosid-2-ulosyl)acetate
CAS No.:1308272-15-2
Molecular Formula:C₃₁H₃₃FO₇
Molecular Weight:536.597
Hs Code.:

Synonyms:ethyl fluoro-2-(3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosid-2-ulosyl)acetate

Suppliers and Price of ethyl fluoro-2-(3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosid-2-ulosyl)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl fluoro-2-(3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosid-2-ulosyl)acetate

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Technology Process of ethyl fluoro-2-(3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosid-2-ulosyl)acetate

There total 1 articles about ethyl fluoro-2-(3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosid-2-ulosyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 883857-57-6
ethyl ethoxythiocarbonylsulfanylfluoroacetate

: 138511-92-9
1,5-anhydro-2,3,4,6-tetra-O-benzyl-D-lyxo-hex-1-enitol

: 1308272-15-2
ethyl fluoro-2-(3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosid-2-ulosyl)acetate

Guidance literature:: With dilauryl peroxide; In 1,2-dichloro-ethane; tert-butyl alcohol; at 95 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201100183

Reference yield: 39.0%

: 1308272-15-2
ethyl fluoro-2-(3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosid-2-ulosyl)acetate

: ethyl 2-fluoro-2-(3,4,6-tri-O-benzyl-α-D-talopyranosyl)acetate

Guidance literature:: With sodium tetrahydroborate; In methanol; at -78 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/chem.201100183

Reference yield:

: 1308272-15-2
ethyl fluoro-2-(3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosid-2-ulosyl)acetate

: 1467598-20-4
ethyl 2-fluoro-2-(3,4,6-tri-O-benzyl-α-D-talopyranosyl)acetate

: 1467598-19-1
ethyl 2-fluoro-2-(3,4,6-tri-O-benzyl-α-D-talopyranosyl)acetate

Guidance literature:: With sodium tetrahydroborate; In methanol; at -78 ℃; for 1.5h; Overall yield = 39 %; Overall yield = 0.083 g; Inert atmosphere;
DOI:10.1002/chem.201302070