allyl 2-(triphenylphosphoranylidene)butanoate

Base Information

Chemical Name:allyl 2-(triphenylphosphoranylidene)butanoate
CAS No.:412328-08-6
Molecular Formula:C₂₅H₂₅O₂P
Molecular Weight:388.446
Hs Code.:

Synonyms:allyl 2-(triphenylphosphoranylidene)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 2-(triphenylphosphoranylidene)butanoate

Chemical Property:

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Technology Process of allyl 2-(triphenylphosphoranylidene)butanoate

There total 2 articles about allyl 2-(triphenylphosphoranylidene)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: (1-allyloxy-1-oxobutan-2-yl)triphenylphosphonium bromide

: 412328-08-6
allyl 2-(triphenylphosphoranylidene)butanoate

Guidance literature:: With sodium hydroxide; In dichloromethane; water; at 0 - 20 ℃; for 2h;
DOI:10.1039/d0ob00958j

Reference yield:

: 6291-97-0
allyl 2-bromobutanoate

: 412328-08-6
allyl 2-(triphenylphosphoranylidene)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2 h / Inert atmosphere; Heating

1.2: 18 h / Inert atmosphere; Reflux

2.1: sodium hydroxide / dichloromethane; water / 2 h / 0 - 20 °C

With sodium hydroxide; In dichloromethane; water;
DOI:10.1039/d0ob00958j