3-t-butyldiphenylsilyloxy-1-{4-[2-(p-nitrobenzyloxycarbonylamino)ethylcarbamoyl]-1,3-thiazol-2-yl}azetidine

Base Information

Chemical Name:3-t-butyldiphenylsilyloxy-1-{4-[2-(p-nitrobenzyloxycarbonylamino)ethylcarbamoyl]-1,3-thiazol-2-yl}azetidine
CAS No.:429671-92-1
Molecular Formula:C₃₃H₃₇N₅O₆SSi
Molecular Weight:659.838
Hs Code.:

Synonyms:3-t-butyldiphenylsilyloxy-1-{4-[2-(p-nitrobenzyloxycarbonylamino)ethylcarbamoyl]-1,3-thiazol-2-yl}azetidine

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Chemical Property of 3-t-butyldiphenylsilyloxy-1-{4-[2-(p-nitrobenzyloxycarbonylamino)ethylcarbamoyl]-1,3-thiazol-2-yl}azetidine

Chemical Property:

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Technology Process of 3-t-butyldiphenylsilyloxy-1-{4-[2-(p-nitrobenzyloxycarbonylamino)ethylcarbamoyl]-1,3-thiazol-2-yl}azetidine

There total 6 articles about 3-t-butyldiphenylsilyloxy-1-{4-[2-(p-nitrobenzyloxycarbonylamino)ethylcarbamoyl]-1,3-thiazol-2-yl}azetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: diethylphosphoryl cyanide

: (2-t-butoxycarbonylaminoethyl)carbamic acid p-nitrobenzyl ester

: 2-(p-nitrobenzyloxycarbonylamino)ethylamine hydrochloride

: 429666-56-8
3-t-butyldiphenylsilyloxy-1-(4-carboxyl-1,3-thiazol-2-yl)azetidine

: 429671-92-1
3-t-butyldiphenylsilyloxy-1-{4-[2-(p-nitrobenzyloxycarbonylamino)ethylcarbamoyl]-1,3-thiazol-2-yl}azetidine

Guidance literature:: With hydrogenchloride; triethylamine; In 1,4-dioxane; N-methyl-acetamide; diethyl ether;

Reference yield:

: 429666-52-4
3-t-butyldiphenylsilyloxy-1-(4-hydroxymethyl-1,3-thiazol-2-yl)azetidine

: 429671-92-1
3-t-butyldiphenylsilyloxy-1-{4-[2-(p-nitrobenzyloxycarbonylamino)ethylcarbamoyl]-1,3-thiazol-2-yl}azetidine

Guidance literature:: Multi-step reaction with 3 steps

1: manganese dioxide / dichloromethane

2: hydrogenchloride / tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol

3: hydrogenchloride; triethylamine / 1,4-dioxane; N-methyl-acetamide; diethyl ether

With hydrogenchloride; manganese dioxide; triethylamine; In tetrahydrofuran; 1,4-dioxane; N-methyl-acetamide; methanol; diethyl ether; dichloromethane; water; ethyl acetate; tert-butyl alcohol;

Reference yield:

: 429673-08-5
3-t-butyldiphenylsilyloxy-1-(4-hydroxymethyl-1,3-oxazol-2-yl)azetidine

: 429671-92-1
3-t-butyldiphenylsilyloxy-1-{4-[2-(p-nitrobenzyloxycarbonylamino)ethylcarbamoyl]-1,3-thiazol-2-yl}azetidine

Guidance literature:: Multi-step reaction with 3 steps

1: manganese dioxide / dichloromethane

2: hydrogenchloride / tetrahydrofuran; dichloromethane; water; tert-butyl alcohol

3: hydrogenchloride; triethylamine / 1,4-dioxane; N-methyl-acetamide; diethyl ether

With hydrogenchloride; manganese dioxide; triethylamine; In tetrahydrofuran; 1,4-dioxane; N-methyl-acetamide; diethyl ether; dichloromethane; water; tert-butyl alcohol;