6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl [methyl(2,3-di-O-benzoyl-4-O-methyl-β-D-glucopyranosyl)uronate]-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranoside

Base Information

Chemical Name:6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl [methyl(2,3-di-O-benzoyl-4-O-methyl-β-D-glucopyranosyl)uronate]-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranoside
CAS No.:898528-07-9
Molecular Formula:C₅₅H₆₈Cl₃NO₂₇
Molecular Weight:1281.49
Hs Code.:

6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl [methyl(2,3-di-O-benzoyl-4-O-methyl-β-D-glucopyranosyl)uronate]-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranoside

Synonyms:6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl [methyl(2,3-di-O-benzoyl-4-O-methyl-β-D-glucopyranosyl)uronate]-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranoside

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Chemical Property of 6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl [methyl(2,3-di-O-benzoyl-4-O-methyl-β-D-glucopyranosyl)uronate]-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranoside

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Technology Process of 6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl [methyl(2,3-di-O-benzoyl-4-O-methyl-β-D-glucopyranosyl)uronate]-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranoside

There total 1 articles about 6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl [methyl(2,3-di-O-benzoyl-4-O-methyl-β-D-glucopyranosyl)uronate]-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4,5-bis-benzoyloxy-3-methoxy-6-(3,4,5-trihydroxy-6-{3,4,5-trihydroxy-6-[6-(2,2,2-trichloro-ethoxycarbonylamino)-hexyloxy]-tetrahydro-pyran-2-ylmethoxy}-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-2-carboxylic acid methyl ester

: 108-24-7
acetic anhydride

: 898528-07-9
6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl [methyl(2,3-di-O-benzoyl-4-O-methyl-β-D-glucopyranosyl)uronate]-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 3h;
DOI:10.1248/cpb.54.485

Reference yield: 76.9%

: 898528-07-9
6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl [methyl(2,3-di-O-benzoyl-4-O-methyl-β-D-glucopyranosyl)uronate]-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranoside

: 898528-08-0
6-aminohexyl [methyl(2,3-di-O-benzoyl-4-O-methyl-β-D-glucopyranosyl)uronate]-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranoside

Guidance literature:: With acetic acid; zinc; at 20 ℃; for 16h;
DOI:10.1248/cpb.54.485

Reference yield:

: 898528-07-9
6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl [methyl(2,3-di-O-benzoyl-4-O-methyl-β-D-glucopyranosyl)uronate]-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-acetyl-β-D-galactopyranoside

: 898528-12-6
C₆₂H₈₂N₂O₃₀

Guidance literature:: Multi-step reaction with 3 steps

1: 76.9 percent / Zn; AcOH / 16 h / 20 °C

2: 92.4 percent / triethylamine; diethyl phosphorocyanidate / dimethylformamide / 16 h / 20 °C

3: 79.8 percent / Zn; AcOH / 1 h / 20 °C

With diethyl cyanophosphonate; acetic acid; triethylamine; zinc; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.54.485