N,N',N''-tris[(1S)-2-methoxy-2-oxy-1-(1-benzylimidazol-4-ylmethyl)]nitrilotriacetamide

Base Information

Chemical Name:N,N',N''-tris[(1S)-2-methoxy-2-oxy-1-(1-benzylimidazol-4-ylmethyl)]nitrilotriacetamide
CAS No.:1318799-04-0
Molecular Formula:C₄₈H₅₄N₁₀O₉
Molecular Weight:915.018
Hs Code.:

Synonyms:N,N',N''-tris[(1S)-2-methoxy-2-oxy-1-(1-benzylimidazol-4-ylmethyl)]nitrilotriacetamide

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Chemical Property of N,N',N''-tris[(1S)-2-methoxy-2-oxy-1-(1-benzylimidazol-4-ylmethyl)]nitrilotriacetamide

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Technology Process of N,N',N''-tris[(1S)-2-methoxy-2-oxy-1-(1-benzylimidazol-4-ylmethyl)]nitrilotriacetamide

There total 2 articles about N,N',N''-tris[(1S)-2-methoxy-2-oxy-1-(1-benzylimidazol-4-ylmethyl)]nitrilotriacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 139-13-9,80751-51-5
nitrilotriacetic acid

: 19817-75-5
N'-benzyl-L-histidine methyl ester

: 1318799-04-0
N,N',N''-tris[(1S)-2-methoxy-2-oxy-1-(1-benzylimidazol-4-ylmethyl)]nitrilotriacetamide

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 14h; pH=7;
DOI:10.1016/j.jinorgbio.2010.07.009

Reference yield:

: 20898-44-6,81018-79-3
Boc-His(Bzl)-OH

: 1318799-04-0
N,N',N''-tris[(1S)-2-methoxy-2-oxy-1-(1-benzylimidazol-4-ylmethyl)]nitrilotriacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 14 h / 0 - 20 °C / pH 7

2: formic acid / 15 h

3: 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 14 h / 0 - 20 °C / pH 7

With 4-methyl-morpholine; formic acid; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1016/j.jinorgbio.2010.07.009