C₄₀H₄₅F₃N₂O₈

Base Information

Chemical Name:C₄₀H₄₅F₃N₂O₈
CAS No.:1315455-22-1
Molecular Formula:C₄₀H₄₅F₃N₂O₈
Molecular Weight:738.801
Hs Code.:

C<sub>40</sub>H<sub>45</sub>F<sub>3</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₄₀H₄₅F₃N₂O₈

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Chemical Property of C₄₀H₄₅F₃N₂O₈

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Technology Process of C₄₀H₄₅F₃N₂O₈

There total 11 articles about C₄₀H₄₅F₃N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1315454-68-2
C₃₈H₄₆N₂O₇

: 407-25-0
trifluoroacetic anhydride

: 1315455-22-1
C₄₀H₄₅F₃N₂O₈

Guidance literature:: With pyridine; at 20 - 50 ℃; for 5h; Inert atmosphere;
DOI:10.1002/chem.201003489

Reference yield:

: C₃₃H₄₅NO₆Si

: 1315455-22-1
C₄₀H₄₅F₃N₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 2.5 h / 20 °C / Inert atmosphere

4: sodium cyanoborohydride / methanol; chloroform-d1 / 5 h / Molecular sieve; Inert atmosphere

5: pyridine / 5 h / 20 - 50 °C / Inert atmosphere

With pyridine; tetrabutyl ammonium fluoride; sodium cyanoborohydride; caesium carbonate; Dess-Martin periodane; acetic acid; In tetrahydrofuran; methanol; chloroform-d1; dichloromethane; N,N-dimethyl-formamide; 3: Dess-Martin oxidation;
DOI:10.1002/chem.201003489

Reference yield:

: 1315454-59-1
C₂₁H₂₃NO₃

: 1315455-22-1
C₄₀H₄₅F₃N₂O₈

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanoborohydride / methanol; chloroform-d1 / 5 h / Molecular sieve; Inert atmosphere

2: pyridine / 5 h / 20 - 50 °C / Inert atmosphere

With pyridine; sodium cyanoborohydride; In methanol; chloroform-d1;
DOI:10.1002/chem.201003489