3-methoxy-4,5-methylenedioxycinnamyl 3',4',5'-trimethoxyphenylpropiolate

Base Information

Chemical Name:3-methoxy-4,5-methylenedioxycinnamyl 3',4',5'-trimethoxyphenylpropiolate
CAS No.:123251-29-6
Molecular Formula:C₂₃H₂₂O₈
Molecular Weight:426.423
Hs Code.:

Synonyms:3-methoxy-4,5-methylenedioxycinnamyl 3',4',5'-trimethoxyphenylpropiolate

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Chemical Property of 3-methoxy-4,5-methylenedioxycinnamyl 3',4',5'-trimethoxyphenylpropiolate

Chemical Property:

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Technology Process of 3-methoxy-4,5-methylenedioxycinnamyl 3',4',5'-trimethoxyphenylpropiolate

There total 6 articles about 3-methoxy-4,5-methylenedioxycinnamyl 3',4',5'-trimethoxyphenylpropiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 4698-21-9
3-(3,4,5-trimethoxyphenyl)propiolic acid

: 69618-94-6
3-(3-methoxy-4,5-methylenedioxyphenyl)-2-(E)-propen-1-ol

: 123251-29-6
3-methoxy-4,5-methylenedioxycinnamyl 3',4',5'-trimethoxyphenylpropiolate

Guidance literature:: With toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In pyridine; for 26h; Ambient temperature;

Reference yield:

: 1878-29-1,30273-65-5,31892-98-5
ethyl (E)-3-(3,4,5-trimethoxyphenyl)acrylate

: 123251-29-6
3-methoxy-4,5-methylenedioxycinnamyl 3',4',5'-trimethoxyphenylpropiolate

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / Br₂ / CHCl₃ / 1 h / 0 °C

2: 56 percent / KOH / H₂O; ethanol / 8 h / Heating

3: 80 percent / p-TSA, DCC / pyridine / 26 h / Ambient temperature

With potassium hydroxide; bromine; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In pyridine; ethanol; chloroform; water;

Reference yield:

: 5780-07-4
3-methoxy-4,5-methylenedioxybenzaldehyde

: 123251-29-6
3-methoxy-4,5-methylenedioxycinnamyl 3',4',5'-trimethoxyphenylpropiolate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / K₂CO₃ / H₂O / 5 h / 85 °C

2: 81 percent / LAH / diethyl ether / 2.5 h / -15 °C

3: 80 percent / p-TSA, DCC / pyridine / 26 h / Ambient temperature

With lithium aluminium tetrahydride; potassium carbonate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In pyridine; diethyl ether; water;