N-benzyloxycarbonyl-6-aminohexyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Base Information

Chemical Name:N-benzyloxycarbonyl-6-aminohexyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside
CAS No.:1415996-61-0
Molecular Formula:C₄₁H₄₅NO₉
Molecular Weight:695.81
Hs Code.:

Synonyms:N-benzyloxycarbonyl-6-aminohexyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

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Chemical Property of N-benzyloxycarbonyl-6-aminohexyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

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Technology Process of N-benzyloxycarbonyl-6-aminohexyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

There total 1 articles about N-benzyloxycarbonyl-6-aminohexyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 460082-41-1
phenyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 1415996-61-0
N-benzyloxycarbonyl-6-aminohexyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -10 ℃; for 5h; Molecular sieve; Inert atmosphere;
DOI:10.1039/c2ob26928g

Reference yield:

: 1415996-61-0
N-benzyloxycarbonyl-6-aminohexyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

: C₃₄H₄₁NO₉

Guidance literature:: With trifluoroacetic acid; In methanol; dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1039/c2ob26928g

Reference yield:

: 1415996-61-0
N-benzyloxycarbonyl-6-aminohexyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

: 1415996-38-1
C₆₂H₆₇Cl₃N₂O₁₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: trifluoroacetic acid / dichloromethane; methanol / 0.5 h / 0 °C

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 6 h / 0 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

4.1: 1,1'-sulfinylbisbenzene; trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine / dichloromethane / -60 - -40 °C / Molecular sieve; Inert atmosphere

4.2: -60 - 20 °C / Inert atmosphere

5.1: thiourea; 2,6-dimethylpyridine / N,N-dimethyl-formamide / 12 h / 50 °C

6.1: 1.3-propanedithiol; triethylamine / tetrahydrofuran; methanol / 48 h / 20 °C

7.1: sodium hydrogencarbonate / water; tetrahydrofuran / 0.17 h / 0 °C

With 2,6-dimethylpyridine; 1.3-propanedithiol; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trifluoromethylsulfonic anhydride; [bis(acetoxy)iodo]benzene; 1,1'-sulfinylbisbenzene; sodium hydrogencarbonate; potassium carbonate; triethylamine; thiourea; trifluoroacetic acid; 2,4,6-tri-tert-butylpyrimidine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26928g