4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hex-2-ynyl acetate

Base Information

Chemical Name:4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hex-2-ynyl acetate
CAS No.:152297-78-4
Molecular Formula:C₁₈H₂₈O₃
Molecular Weight:292.419
Hs Code.:

Synonyms:4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hex-2-ynyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hex-2-ynyl acetate

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Technology Process of 4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hex-2-ynyl acetate

There total 3 articles about 4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hex-2-ynyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 108-24-7
acetic anhydride

: 152297-77-3
4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hex-2-yne-1,4-diol

: 152297-78-4
4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hex-2-ynyl acetate

Guidance literature:: With triethylamine; at 25 ℃; for 0.25h;
DOI:10.1002/hlca.200490155

Reference yield: 97.0%

: 152297-78-4
4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hex-2-ynyl acetate

Guidance literature:

Reference yield:

: 17283-81-7
4-(2,6,6-Trimethyl-cyclohex-1-enyl)-butan-2-on

: 152297-78-4
4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hex-2-ynyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / KOH / tetrahydrofuran / 3.5 h / 15 °C

2: 97 percent / Et₃N / 0.25 h / 25 °C

With potassium hydroxide; triethylamine; In tetrahydrofuran;
DOI:10.1002/hlca.200490155