2,3-butanedione bis[(8-bis(p-trifluoromethyl)phenylnaphthylimino)acenaphthene]

Base Information

Chemical Name:2,3-butanedione bis[(8-bis(p-trifluoromethyl)phenylnaphthylimino)acenaphthene]
CAS No.:1609159-02-5
Molecular Formula:C₃₈H₂₆F₆N₂
Molecular Weight:624.628
Hs Code.:

Synonyms:2,3-butanedione bis[(8-bis(p-trifluoromethyl)phenylnaphthylimino)acenaphthene]

Suppliers and Price of 2,3-butanedione bis[(8-bis(p-trifluoromethyl)phenylnaphthylimino)acenaphthene]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-butanedione bis[(8-bis(p-trifluoromethyl)phenylnaphthylimino)acenaphthene]

Chemical Property:

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Technology Process of 2,3-butanedione bis[(8-bis(p-trifluoromethyl)phenylnaphthylimino)acenaphthene]

There total 4 articles about 2,3-butanedione bis[(8-bis(p-trifluoromethyl)phenylnaphthylimino)acenaphthene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 8-(4-(trifluoromethyl)phenyl)naphthalen-1-amine

: 431-03-8
dimethylglyoxal

: 1609159-02-5
2,3-butanedione bis[(8-bis(p-trifluoromethyl)phenylnaphthylimino)acenaphthene]

Guidance literature:: With formic acid; In methanol; at 20 ℃; Reflux; Inert atmosphere;
DOI:10.1021/ja502130w

Reference yield:

: 455-13-0
4-Iodobenzotrifluoride

: 1609159-02-5
2,3-butanedione bis[(8-bis(p-trifluoromethyl)phenylnaphthylimino)acenaphthene]

Guidance literature:: Multi-step reaction with 3 steps

1: silver(I) acetate; palladium diacetate / 40 h / 140 °C / Inert atmosphere

2: potassium hydroxide; water / ethanol / 38 h / 130 °C / Inert atmosphere

3: formic acid / methanol / 20 °C / Reflux; Inert atmosphere

With formic acid; water; silver(I) acetate; palladium diacetate; potassium hydroxide; In methanol; ethanol;
DOI:10.1021/ja502130w

Reference yield:

: N-{8-[4-(trifluoromethyl)phenyl]naphthalen-1-yl}pyridine-2-carboxamide

: 1609159-02-5
2,3-butanedione bis[(8-bis(p-trifluoromethyl)phenylnaphthylimino)acenaphthene]

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide; water / ethanol / 38 h / 130 °C / Inert atmosphere

2: formic acid / methanol / 20 °C / Reflux; Inert atmosphere

With formic acid; water; potassium hydroxide; In methanol; ethanol;
DOI:10.1021/ja502130w