(-)-β-D-carbocyclic-1'-(9H-{N²-isobutyryl-O⁶-[p-(nitropheny)ethyl]-guanin-9-yl})-2',3'-O-isopropylidene-5'-O-(tert-butyldimethylsilyl) ribonucleoside

Base Information

• Chemical Name: (-)-β-D-carbocyclic-1'-(9H-{N²-isobutyryl-O⁶-[p-(nitropheny)ethyl]-guanin-9-yl})-2',3'-O-isopropylidene-5'-O-(tert-butyldimethylsilyl) ribonucleoside
• CAS No.: 250699-05-9
• Molecular Formula: C₃₂H₄₆N₆O₇Si
• Molecular Weight: 654.839

Synonyms:(-)-β-D-carbocyclic-1'-(9H-{N²-isobutyryl-O⁶-[p-(nitropheny)ethyl]-guanin-9-yl})-2',3'-O-isopropylidene-5'-O-(tert-butyldimethylsilyl) ribonucleoside

Chemical Property of (-)-β-D-carbocyclic-1'-(9H-{N²-isobutyryl-O⁶-[p-(nitropheny)ethyl]-guanin-9-yl})-2',3'-O-isopropylidene-5'-O-(tert-butyldimethylsilyl) ribonucleoside

Chemical Property:

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Technology Process of (-)-β-D-carbocyclic-1'-(9H-{N²-isobutyryl-O⁶-[p-(nitropheny)ethyl]-guanin-9-yl})-2',3'-O-isopropylidene-5'-O-(tert-butyldimethylsilyl) ribonucleoside

There total 1 articles about (-)-β-D-carbocyclic-1'-(9H-{N²-isobutyryl-O⁶-[p-(nitropheny)ethyl]-guanin-9-yl})-2',3'-O-isopropylidene-5'-O-(tert-butyldimethylsilyl) ribonucleoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(1S,2S,3R,4S)-4-t-butyldimethylsiloxymethyl-2,3-isopropylidenedioxycyclopentanol (135486-55-4) + N2-Isobutyryl-O6-[2-(4-nitrophenylethyl)]guanine (143325-60-4) → (-)-β-D-carbocyclic-1'-(9H-{N2-isobutyryl-O6-[p-(nitropheny)ethyl]-guanin-9-yl})-2',3'-O-isopropylidene-5'-O-(tert-butyldimethylsilyl) ribonucleoside (250699-05-9)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; at 25 ℃; for 12h;

DOI:10.1080/07328319908044853

upstream raw materials:

(1S,2S,3R,4S)-4-t-butyldimethylsiloxymethyl-2,3-isopropylidenedioxycyclopentanol

N²-Isobutyryl-O⁶-[2-(4-nitrophenylethyl)]guanine

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