bis-{2,4,6-tri-O-acetyl-3-deoxy-3-[4-(phenyl)-1H-1,2,3-triazol-1-yl]-β-D-galactopyranosyl}sulfane

Base Information

• Chemical Name: bis-{2,4,6-tri-O-acetyl-3-deoxy-3-[4-(phenyl)-1H-1,2,3-triazol-1-yl]-β-D-galactopyranosyl}sulfane
• CAS No.: 1421638-21-2
• Molecular Formula: C₄₀H₄₄N₆O₁₄S
• Molecular Weight: 864.887
• Mol file: 1421638-21-2.mol

Synonyms:bis-{2,4,6-tri-O-acetyl-3-deoxy-3-[4-(phenyl)-1H-1,2,3-triazol-1-yl]-β-D-galactopyranosyl}sulfane

Chemical Property of bis-{2,4,6-tri-O-acetyl-3-deoxy-3-[4-(phenyl)-1H-1,2,3-triazol-1-yl]-β-D-galactopyranosyl}sulfane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis-{2,4,6-tri-O-acetyl-3-deoxy-3-[4-(phenyl)-1H-1,2,3-triazol-1-yl]-β-D-galactopyranosyl}sulfane

There total 1 articles about bis-{2,4,6-tri-O-acetyl-3-deoxy-3-[4-(phenyl)-1H-1,2,3-triazol-1-yl]-β-D-galactopyranosyl}sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2,2‘,4,4’,5,5‘,6,6‘-hexa-O-acetyl-3,3‘-diazido-3,3‘-dideoxy-1,1‘-sulfanediyl-di-β-D-galactopyranoside (1193784-38-1) + phenylacetylene (536-74-3) → bis-{2,4,6-tri-O-acetyl-3-deoxy-3-[4-(phenyl)-1H-1,2,3-triazol-1-yl]-β-D-galactopyranosyl}sulfane (1421638-21-2)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; at 80 ℃; for 0.666667h; Microwave irradiation;

DOI:10.1021/jm301677r

Reference yield:

bis-{2,4,6-tri-O-acetyl-3-deoxy-3-[4-(phenyl)-1H-1,2,3-triazol-1-yl]-β-D-galactopyranosyl}sulfane (1421638-21-2) → bis-{3-deoxy-3-[4-(phenyl)-1H-1,2,3-triazol-1-yl]-β-D-galactopyranosyl} sulfane (1421638-24-5)

Guidance literature:

With methanol; sodium methylate; for 2.5h;

DOI:10.1021/jm301677r

upstream raw materials:

2,2‘,4,4’,5,5‘,6,6‘-hexa-O-acetyl-3,3‘-diazido-3,3‘-dideoxy-1,1‘-sulfanediyl-di-β-D-galactopyranoside

phenylacetylene

Downstream raw materials:

bis-{3-deoxy-3-[4-(phenyl)-1H-1,2,3-triazol-1-yl]-β-D-galactopyranosyl} sulfane