11-(4-diphenylaminophenyl)dipyrido[3,2-a:2′,3′-c]phenazine

Base Information

• Chemical Name: 11-(4-diphenylaminophenyl)dipyrido[3,2-a:2′,3′-c]phenazine
• CAS No.: 1541809-17-9
• Molecular Formula: C₃₆H₂₃N₅
• Molecular Weight: 525.612
• Mol file: 1541809-17-9.mol

Synonyms:11-(4-diphenylaminophenyl)dipyrido[3,2-a:2′,3′-c]phenazine

Chemical Property of 11-(4-diphenylaminophenyl)dipyrido[3,2-a:2′,3′-c]phenazine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 11-(4-diphenylaminophenyl)dipyrido[3,2-a:2′,3′-c]phenazine

There total 7 articles about 11-(4-diphenylaminophenyl)dipyrido[3,2-a:2′,3′-c]phenazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

11-bromodipyrido[3,2-a:2′,3′-c]phenazine (853914-88-2) + 4-(diphenylamino)phenyl boronic acid (201802-67-7) → 11-(4-diphenylaminophenyl)dipyrido[3,2-a:2′,3′-c]phenazine (1541809-17-9)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In ethanol; water; toluene; Reflux; Inert atmosphere;

DOI:10.1021/ic402082m

Reference yield: 39.0%

1,10-phenanthroline-5,6-dione (27318-90-7) + 5-(4-diphenylaminophenyl)benzo[c][1,2,5]thiadiazole → 11-(4-diphenylaminophenyl)dipyrido[3,2-a:2′,3′-c]phenazine (1541809-17-9)

Guidance literature:

5-(4-diphenylaminophenyl)benzo[c][1,2,5]thiadiazole; With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 15h; Inert atmosphere;

1,10-phenanthroline-5,6-dione; In ethanol; for 15h; Reflux;

DOI:10.1021/acs.inorgchem.6b01039

Reference yield:

1,10-phenanthroline-5,6-dione (27318-90-7) + N4',N4'-diphenyl-[1,1'-biphenyl]-3,4,4'-triamine → 11-(4-diphenylaminophenyl)dipyrido[3,2-a:2′,3′-c]phenazine (1541809-17-9)

Guidance literature:

In ethanol; at 80 ℃; for 48h;

upstream raw materials:

11-bromodipyrido[3,2-a:2′,3′-c]phenazine

4-(diphenylamino)phenyl boronic acid

1,10-phenanthroline-5,6-dione

4-Bromo-benzene-1,2-diamine