Technology Process of 2-phenyl-5-(2-(piperidin-1-yl)ethyloxy)-1,10-phenanthroline
There total 3 articles about 2-phenyl-5-(2-(piperidin-1-yl)ethyloxy)-1,10-phenanthroline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
5-(2-(piperidin-1-yl)ethyloxy)-1,10-phenanthroline; phenyllithium;
In
dibutyl ether; toluene;
at 0 ℃;
for 3h;
Inert atmosphere;
With
manganese(IV) oxide;
In
methanol; dibutyl ether; toluene;
for 24h;
DOI:10.1002/chem.201202990
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide / dimethyl sulfoxide / 4 h / 60 °C / Inert atmosphere
2.1: toluene; dibutyl ether / 3 h / 0 °C / Inert atmosphere
2.2: 24 h
With
potassium hydroxide;
In
dibutyl ether; dimethyl sulfoxide; toluene;
DOI:10.1002/chem.201202990
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide / dimethyl sulfoxide / 4 h / 60 °C / Inert atmosphere
2.1: toluene; dibutyl ether / 3 h / 0 °C / Inert atmosphere
2.2: 24 h
With
potassium hydroxide;
In
dibutyl ether; dimethyl sulfoxide; toluene;
DOI:10.1002/chem.201202990
