Technology Process of C23H32O5Si
There total 5 articles about C23H32O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylsilane; Wilkinson's catalyst;
In
toluene;
at 20 - 60 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1002/asia.201300362
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 6 h / 20 °C / Inert atmosphere
2: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere
3: triethylsilane; Wilkinson's catalyst / toluene / 1.5 h / 20 - 60 °C / Inert atmosphere
With
triethylsilane; Wilkinson's catalyst; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dichloromethane; dimethyl sulfoxide; toluene;
2: |Wittig Olefination;
DOI:10.1002/asia.201300362
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 9 h / -5 - 5 °C / Inert atmosphere
2: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 0 °C / Inert atmosphere
3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 6 h / 20 °C / Inert atmosphere
4: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere
5: triethylsilane; Wilkinson's catalyst / toluene / 1.5 h / 20 - 60 °C / Inert atmosphere
With
triethylsilane; Wilkinson's catalyst; tetra-(n-butyl)ammonium iodide; sodium hydride; pyridine hydrogenfluoride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; pyridine; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
4: |Wittig Olefination;
DOI:10.1002/asia.201300362
