Technology Process of C23H30N4O3
There total 5 articles about C23H30N4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 15h;
DOI:10.1016/j.bmcl.2012.06.059
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C
2: water; sodium hydroxide / 2 h / Reflux
3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 15 h / 20 °C
With
dmap; water; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.06.059
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium azide; tetrabutylammomium bromide; potassium iodide / toluene / 6 h / Reflux
2: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C
3: water; sodium hydroxide / 2 h / Reflux
4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 15 h / 20 °C
With
dmap; sodium azide; tetrabutylammomium bromide; water; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium iodide; sodium hydroxide;
In
N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2012.06.059