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C28H36O5

Base Information
  • Chemical Name:C28H36O5
  • CAS No.:1187655-92-0
  • Molecular Formula:C28H36O5
  • Molecular Weight:452.591
  • Hs Code.:
C<sub>28</sub>H<sub>36</sub>O<sub>5</sub>

Synonyms:C28H36O5

Suppliers and Price of C28H36O5
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Chemical Property of C28H36O5
Chemical Property:
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Technology Process of C28H36O5

There total 10 articles about C28H36O5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 15h;
Guidance literature:
Multi-step reaction with 7 steps
1.1: n-butyllithium / tetrahydrofuran; hexanes / 0.58 h / -78 °C
1.2: -78 °C
2.1: dihydrogen peroxide / Shi's ketone / ethanol; dichloromethane; water; acetonitrile / 9 h / 0 °C / aq buffer (2 M K2CO3 and 4 mM EDTA)
3.1: boron trifluoride diethyl etherate / dichloromethane / 0.12 h / -78 °C
4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 18.5 h / 20 °C
5.1: potassium hydroxide / ethanol / 2 h / 20 °C
6.1: methanol; sodium tetrahydroborate; cerium(III) chloride heptahydrate / 0.33 h / 20 °C
7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C
With methanol; sodium tetrahydroborate; n-butyllithium; tetrapropylammonium perruthennate; cerium(III) chloride heptahydrate; boron trifluoride diethyl etherate; dihydrogen peroxide; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; potassium hydroxide; Shi's ketone; In tetrahydrofuran; hexanes; ethanol; dichloromethane; water; acetonitrile;
Guidance literature:
Multi-step reaction with 7 steps
1.1: n-butyllithium / tetrahydrofuran; hexanes / 0.58 h / -78 °C
1.2: -78 °C
2.1: dihydrogen peroxide / Shi's ketone / ethanol; dichloromethane; water; acetonitrile / 9 h / 0 °C / aq buffer (2 M K2CO3 and 4 mM EDTA)
3.1: boron trifluoride diethyl etherate / dichloromethane / 0.12 h / -78 °C
4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 18.5 h / 20 °C
5.1: potassium hydroxide / ethanol / 2 h / 20 °C
6.1: methanol; sodium tetrahydroborate; cerium(III) chloride heptahydrate / 0.33 h / 20 °C
7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C
With methanol; sodium tetrahydroborate; n-butyllithium; tetrapropylammonium perruthennate; cerium(III) chloride heptahydrate; boron trifluoride diethyl etherate; dihydrogen peroxide; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; potassium hydroxide; Shi's ketone; In tetrahydrofuran; hexanes; ethanol; dichloromethane; water; acetonitrile;
upstream raw materials:

C26H32O4

chloromethyl methyl ether

trans-geranyl bromide

C11H15BrO4

Downstream raw materials:

C21H30O6

C28H38O7

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